DOI QR코드

DOI QR Code

The research about the physical properties and flexural strength changed by Low Temperature Degradation of TZP monolithic all-ceramic crown block to make bio-prosthetic dentistry

치과용 생체보철물 제작을 위한 TZP 단일구조 전부도재관 블럭의 물성과 저온열화 후 굴곡강도에 관한 연구

  • Received : 2012.04.30
  • Accepted : 2012.06.26
  • Published : 2012.06.30

Abstract

Purpose: The objective of this study is to find out physical properties and the flexural strength changed by the low temperature degradation of the block which is needed to make bio-prosthetic dentistry which is better than feldspar affiliated ceramic made by building up ceramic powder and also to apply this to the clinical use of zirconia monolithic all-ceramic crown. Methods: Flexural strength of each sample was evaluated before and after the Low Temperature Degradation, and physical properties of the Tetra Zirconia Block containing 3mol % was evaluated as well. The average and standard deviation of each experimental group were came out of the evaluation. Statistical package for social science 18.0 was used for statistics. Results: The average density of the monolithic all-ceramic crown was $6.0280{\pm}0.0147g/cm$, the relative density was 99.01 %. When the sample was sintered at $1480^{\circ}C$ the diameter of average particle was $396.62{\pm}33.71nm$. All the samples had no monolithic peak after XRD evaluation but only had tetragonal peak. There were statistically significant differences in the result of flexural strength of the samples evaluated after and before the low temperature degradation, the flexural strength before the low temperature degradation was $1747.40{\ss}{\acute{A}}$, at the temperature of $130^{\circ}C$ the flexural strength after the low temperature degradation was 1063.99MPa (p<0.001). There was statistically significant difference in the result of strength of 1020.07MPa after the low temperature degradation at the temperature of $200^{\circ}C$ (p<0.001). Conclusion: The block which was made for this evaluation possesses such an excellent strength among dental restorative materials that it is thought to have no problems to use for tetragonal zirconia polycrystal.

Keywords

References

  1. 박재홍, 황정원, 신상완. 수종 지르코니아 세라믹의 굴곡 강도에 관한 연구. 대한치과보철학회지, 42(2), 142-153, 2004.
  2. 배태성. CAD/CAM 지르코니아 재료의 특성. 대한치과의사협회지, 49(5), 260-264, 2011.
  3. 식약청. 식약청고시 제 2010-91호.
  4. 식약청. 지르코니아 소재 치과재료의 평가 가이드라인. 2011.
  5. 정형호. 치아수복용 $t-ZrO_{2}/Al_{2}O_{3}-Fe_{2}O_{3}$ 복합체 CAD/CAM block의 기계적 및 광학적 특성. 고려대학교 공학대학원 석사학위논문, 2006.
  6. 정효경, 곽동주. Full Zirconia Crown용으로 사용되는 block의 제조사의 굴곡강도와 임상작업후의 굴곡 강도에 관한 연구. 대한치과기공학회지, 33(4), 283-289, 2011.
  7. Anusavice K. Phillip's Science of Dental Materials. 11, St. Louis: Saunders, 337-348, 583-618, 2003.
  8. Ardlin BI. Transformation-toughened zirconia for dental inlays, crowns and bridges: chemical stability and effect of low-temperature aging on flexural strength and surface structure. Dental Materials, 18(8), 590-595, 2002. https://doi.org/10.1016/S0109-5641(01)00095-1
  9. Ban S, Sato H, Suehiro Y, Nakanishi H, Nawa M. Biaxial flexure strength and low temperature degradation of Ce-TZP/$Al_{2}O_{3}$ nanocomposite and Y-TZP as dental restoratives. J Biomedical Materials Research Part B: Applied Biomaterials, 87B(2), 492-498, 2008. https://doi.org/10.1002/jbm.b.31131
  10. Campbell SD, Sozio RB. Evaluation of the fit and strength of an all-ceramic fixed partial denture. 59(3), 301-306, 1988. https://doi.org/10.1016/0022-3913(88)90177-1
  11. Chen HY, Hickel R, Setcos JC, Kunzelmann KH. Effects of surface finish and fatigue testing on the fracture strength of CAD-CAM and pressed-ceramic crowns. J Prosthetic Dentistry, 82(4), 468-475, 1999. https://doi.org/10.1016/S0022-3913(99)70036-3
  12. Chevalier J. What future for zirconia as a biomaterial?. Biomatetials, 27(4), 535-543, 2006.
  13. Christel P, Meunier A, Heller M, Torre JP, Peille CN. Mechanical properties and short-term in vivo evaluation of yttrium-oxide-partially-stabilized zirconia. J Biomedical Materials Research, 23(1), 45-61, 1989. https://doi.org/10.1002/jbm.820230105
  14. Coornaert J, Adriaens P, De Boever. Long-term clinical study of porcelain-fused-to-gold restorations. J Prosthetic Dentistry, 51(3), 338-342, 1984. https://doi.org/10.1016/0022-3913(84)90217-8
  15. Denry I, Kelly JR. State of the art of zirconia for dental applications. Dental Materials, 24(3), 299-307, 2008. https://doi.org/10.1016/j.dental.2007.05.007
  16. Gomes AL, Montero J, Zirconia implant abutments: A review. Medicina Oral Patologia Oral Cirugia Bucal, 16(1), e50-e55, 2011.
  17. Guazzato M, Albakry M, Ringer SP, Swain MV. Strength, fracture toughness and microstructure of a selection of all-ceramic materials. Part II. Zirconia-based dental ceramics. Dental Materials, 20(5), 449-456, 2004. https://doi.org/10.1016/j.dental.2003.05.002
  18. ISO 6872. Dentistry : Ceramic materials. 2008.
  19. ISO 10993-5. Describes test methods to assess the in vitro cytotoxicity of medical devices. 2009.
  20. ISO 10993-10. Describes the procedure for the assessment of medical devices and their constituent materials with regard to their potential to produce irritation and skin sensitization. 2010.
  21. ISO 10993-11. Specifies requirements and gives guidance on procedures to be followed in the evaluation of the potential for medical device materials to cause adverse systemic reactions. 2006.
  22. Kelly JR, Nishimura I, campbell SD. Ceramics in dentistry: Historical roots and current perspectives. J Prosthetic Dentistry, 75(1), 18-32, 1996. https://doi.org/10.1016/S0022-3913(96)90413-8
  23. Kim DJ. Effect of $Ta_{2}O_{5}$, $Nb_{2}O_{5}$, and $HfO_{2}$ Alloying on the Transformability of $Y_{2}O_{3}$-Stabilized Tetragonal $ZnO_{2}$, J American Ceramic Society, 73(1), 115-120, 1990. https://doi.org/10.1111/j.1151-2916.1990.tb05100.x
  24. Matsul M, Soma T, Oda I. Effect of Microstructure on Strengh of Y-TZP Components, Advances in Ceramics, Science and Technology of Zirconia II. American Ceramic Society, 12, 371, 1984.
  25. Masaki T. Mechanical properties of Y-PSZ after aging at low temperature, International Journal of High Technology Ceramics, 2(2), 85-98, 1986. https://doi.org/10.1016/0267-3762(86)90011-1
  26. Miyazaki T, Hotta Y, Kunii J, Kuriyama S, Tamaki Y. A review of dental CAD/CAM: current status and future perspectives from 20 years of experience. Dental Material Journal, 28(1), 44-56, 2009. https://doi.org/10.4012/dmj.28.44
  27. Nakamura K, Kanno T, Milleding P, Ortengren U. Zirconia as a dental implant abutment material: a systematic review. International Journal of Prosthodontics, 23(4), 299-309, 2010.
  28. Nakamura T, Ohyama T, Imanishi A, Nakamura T, Ishigaki S. Fracture resistance of pressable glass-ceramic fixed partial dentures. J Oral Rehabilitation, 29(10), 951-955, 2002. https://doi.org/10.1046/j.1365-2842.2002.00929.x
  29. Piconi C, Maccauro G. Zirconia as a ceramic biomaterial. Biomaterials, 20, 1-25, 1999. https://doi.org/10.1016/S0142-9612(98)00010-6
  30. Piddock V, Qualtrough AJE. Dental ceramics-an update. J Dentistry, 18(5), 227-235, 1990. https://doi.org/10.1016/0300-5712(90)90019-B
  31. Powers J, Sakaguchi R. Craig's Restorative Dental Materials. 12th Ed., St. Louis, MO, Mosby, 444-464, 2006.
  32. Rieth PH, Reed JS, Naumann AW. Fabrication and flexural strength of ultrafine -grained yttria-stabilized zirconia. Am Ceram Soc Bull, 55(8), 717-721, 1976.
  33. Sato T, Shimada M, Crystalline Phase Change in Yttria-Partially-Stabilized Zirconia by Low-Temperature Annealing. J American Ceramic Society, 67(10), C212-C213, 1984.
  34. Sato T, Shimada M. Transformation of Yttria-Doped Tetragonal $ZrO_{2}$ Polycrystals by Annealing in Water. J American Ceramic Society, 68(6), 356, 1985. https://doi.org/10.1111/j.1151-2916.1985.tb15239.x
  35. Sobrinho LC, Cattell MJ, Glover RH, Knowles JC. Investigation of the dry and wet fatigue properties of three all-ceramic crown systems. Int J Prosthodont, 11(3), 255-262, 1998.
  36. Watanabe M, Iio S, Fukuura I. Aging Behavior of Y-TZP, Advances in Ceramics, Science and Technology of Zirconia II. American Ceramic Society, 12, 391-398, 1984.
  37. Weinstein M, Weinstein LK, Katz S, Weinstein AB. Fused porcelain-to-metal teeth. US Patent, 3,052,983, 1962.
  38. Yamamoto M. Metal ceramics. Quintessence, 219-291, 1987.