Journal of the Mineralogical Society of Korea (한국광물학회지)

The Mineralogical Society of Korea (한국광물학회)
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Quantitative Characterization of Mineral Matters in Coal using a SEM-Based Automated Mineralogy

주사전자현미경 기반 자동광물분석기에 의한 석탄 내 광물함량의 정량분석

  • Lee, Su-Jeong (Mineral Resource Research Division, Korea Institute of Geoscience and Mineral Resources) ;
  • Jung, Steve (Newcrest Mining Limited) ;
  • Kim, Byoung-Gon (Mineral Resource Research Division, Korea Institute of Geoscience and Mineral Resources)
  • 이수정 (한국지질자원연구원 광물자원연구본부) ;
  • ;
  • 김병곤 (한국지질자원연구원 광물자원연구본부)
  • Received : 2011.11.25
  • Accepted : 2011.12.13
  • Published : 2011.12.31
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References

  1. Allen, R.M., Carling, R.W., and VanderSande, J.B. (1986) Microstructural changes in coal during low temperature ashing. Fuel, 65, 321-326. https://doi.org/10.1016/0016-2361(86)90290-5
  2. Anthony, J.W., Bideaux, R.A., Bladh, K.W., and Nichols, M.C. (1995, 1997, 2000, 2003) Handbook of Mineralogy. Mineral Data Publishing.
  3. Cohen, D.R. and Ward, C.R. (1991) SEDNORM - a program to calculate a normative mineralogy for sedimentary rocks based on chemical analyses. Comput. Geosci., 17, 1235-1253. https://doi.org/10.1016/0098-3004(91)90026-A
  4. Creelman, R.A. and Ward, C.R. (1996) A scanning electron microscope method for automated, quantitative analysis of mineral matter in coal. Internaltional Journal of Coal Geology, 30, 249-269. https://doi.org/10.1016/0166-5162(95)00043-7
  5. Du, G., Zhuang, X., Querol, X., Izquierdo, M., Alastuey, A., Moreno, T., and Font, O. (2009) Ge distribution in the Wulantuga high-germanium coal deposit in the Shengli coalfield, Inner Mongolia, Northeastern China. International Journal of Coal Geology, 78, 16-26. https://doi.org/10.1016/j.coal.2008.10.004
  6. French, D., Taylor, J., Dale, L., and Matulis, C. (2001) Quantitative X-ray diffraction analysis of mineral matter in raw coals. Proceedings of 18th Pittsburgh International Coal conference, Newcastle, Australia, December, 2001, 13p.
  7. Galbreath, K., Zygarlicke, C., Casuccio, G., Moore, T., Gottlieb, P., Agron-Olshina, N., Huffman, G., Shah, A., Yang, N., Vleeskens, and Hamburg, G. (1996) Collaborative study of quantitative coal mineral matter analysis using computer-controlled scanning electron microscopy. Fuel, 75, 424-430. https://doi.org/10.1016/0016-2361(95)00277-4
  8. Given, P.H. and Yarzab, R.F. (1978) Analysis of the organic substance of coals: problems posed by the presence of mineral matter. In : Karr, C. (ed.), Analytical Methods for Coal and Coal Products, Volume II, Academic Press, New York., 3-41.
  9. Gluskoter, H.J. (1965) Electronic low-temperature ashing of bituminous coal. Fuel, 44, 285-291.
  10. Gupta, R.P., Wall, T.F., Kajigaya, I., Miyamae, S., and Tsumita, Y. (1998) Computer-controlled scanning electron microscopy of minerals in coal. Progress in Energy Combustion Science, 24, 523-543.
  11. Gupta., R.P., Yan, L., Kennedy, E.M., Wall, T.F., Masson, M., and Kerrison, K. (1999) System Accuracy for CCSEM Analysis of Minerals in Coal. In: Gupta, R.P., Wall, T. and Baxter, L. (eds.) Impact of Mineral Impurities in Solid Fuel Combustion, Kluwer Academic, Plenum Publishers, New York, 225-235.
  12. Gurba, L.W. and Ward, C.R. (2000) Elemental composition of coal macerals in relation to vitrinite reflectance, Gunnedah Basin, Australia, as determined by electron microprobe analysis. International Journal of Coal Geology, 44, 127-147. https://doi.org/10.1016/S0166-5162(00)00007-0
  13. Hicks, D. and Nagelschmidt, G. (1943) The chemical and X-ray diffraction analysis of the roof and clod from some Sough Wales seams and of the mineral matter in the coal. Medical Research Council Special Report, 244, 153-185.
  14. Kok, M.V., Pokol, G., Keskin, C., Madarάsz, and Bagci., S. (2004) Combustion characteristics of lignite and oil shale samples by thermal analysis techniques. Jounral of thermal Analysis and Calorimetry, 76, 247-254. https://doi.org/10.1023/B:JTAN.0000027823.17643.5b
  15. Mastalerz, M. and Bustin, R.M. (1993a) Variation in elemental composition of macerals; an example of the application of electron microprobe to coal studies. International Journal of Coal Geology, 22, 83-99. https://doi.org/10.1016/0166-5162(93)90039-D
  16. Mastalerz, M. and Bustin, R.M. (1993b) Electron microprobe and micro-FTEI analyses applied to maceral chemistry. International Journal of Coal Geology, 24, 333-345. https://doi.org/10.1016/0166-5162(93)90018-6
  17. Painter, P.C., Rimmer, S.M., Snyder, R.W., and Davis, A. (1981) A Fourier transform infra-red study of mineral matter in coal: the application of a leastsquares curve-fitting program. Applied Spectroscopy, 35, 102-106. https://doi.org/10.1366/0003702814731932
  18. Parr, S.W. (1928) The classification of coal. University of Illinois Engineering Experimental Station, Bulletin, 180, 62p.
  19. Straszheim, W.E., Joukin, K.A., Greer, R.T., and Markuszewski, R. (1988) Mounting materials for automated image analysis of coal using backscattered electron imaging. Scanning Electron Microscopy 2, 1257-1264.
  20. Straszheim, W.E. and markuszewski, R. (1992) SEMAIA measurement of the association of mineral matter with the organic coal matrix for predicting fine coal cleanability. Coal Preparation, 10, 59-75. https://doi.org/10.1080/07349349208905193
  21. Suarez-Ruiz, I. and Ward, C.R. (2008) Basic factors controlling coal quality and technological behavior of coal. In: Suarez-Ruiz, I and Crelling, J.C. (eds), Applied coal petrology: the role of petrology in coal utilization: New York, Academic Press, p. 19-59.
  22. Ward, C.R. (1974) Isolation of mineral matter from Australian bituminous coals using hydrogen peroxide. Fuel, 53, 220-221. https://doi.org/10.1016/0016-2361(74)90015-5
  23. Ward, C.R. and French, D. (2003) Evaluation of glass content and estimation of glass composition in fly ash using quantitative X-ray diffractometry. In: Proceedings of the 12th International Conference on Coal Science, Cairns, Australia.
  24. Warne, S.St. J. (1964) Identification and evaluation of minerals in coal by differential thermal analysis. Journal of the Institute of Fuel, 38, 207-217.
  25. Warne, S.St.J. (1975) An improved differential thermal analysis method for the identification of calcite, dolomite and ankerite in coal. Journal of the Institute of Fuel, 50, 142-145.
  26. Wigley, F. and Williamson, J. (1998) Modelling fly ash generation for pulverized coal com- bustion. Progress in Energy and Combustion Science, 24, 337-343.
  27. Wigley, F., Williamson, J., and Gibb, W.H. (1997) The distribution of mineral matter in pulverized coal particles in relation to burnout behaviour. Fuel 76, 1283-1288. https://doi.org/10.1016/S0016-2361(97)00139-7
  28. Van Alphen, C. (2007) Automated mineralogical analysis of coal and ash products - Challenges and requirements. Minerals Engineering, 20, 496-505. https://doi.org/10.1016/j.mineng.2006.12.013
  29. Van Geet, M., Swennen, R., and David, P. (2001) Quantitative coal characterization by means of microfocus X-ray computer tomography, colour image analysis and back scattered scanning electron microscopy. Interna- tional Journal of Coal Geology, 46, 11-25. https://doi.org/10.1016/S0166-5162(01)00006-4
  30. Vassilev, S.V. and Tascon, J.M.D. (2003) Methods for characterization of inorganic and mineral matter in coal: A critical overview. Energy & Fuels, 17, 271-281. https://doi.org/10.1021/ef020113z
  31. Vassilev, S.V., Kitano, K., Takeda, S., and Tsurure, T. (1995) Influence of mineral and chemical composition of coal ashes on their fusibility. Fuel Processing Technology, 45, 27-51. https://doi.org/10.1016/0378-3820(95)00032-3
  32. Zhang, L. and Ninomiya, Y. (2006) Emission of particulate matter from coal combustion and its correlation with coal mineral properties. Fuel, 86, 194-203.
  33. Zhuang, X., Querol, X., Alastuey, A., Juan, R., Plana, F., Lopez-Soler, A., Du, G., and Martynov, V.V. (2006) Geochemistry and mineralogy of the Cretaceous Wulantuga high-germanium coal deposit in Shengli coal field, Inner Mongolia, Northeaster China. International Journal of Coal Geology, 66, 119-136. https://doi.org/10.1016/j.coal.2005.06.005