Bulletin of the Korean Chemical Society

  • 제31권1호
  • /
  • Pages.35-40
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  • 2010
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  • 0253-2964(pISSN)
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  • 1229-5949(eISSN)
대한화학회 (Korean Chemical Society)
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Detection of Small Neutral Carbohydrates Using Various Supporting Materials in Laser Desorption/Ionization Mass Spectrometry

  • Yang, Hyo-Jik (Department of Chemistry, Chungnam National University) ;
  • Lee, Ae-Ra (Department of Chemistry, Chungnam National University) ;
  • Lee, Myung-Ki (Department of Materials Science and Engineering, Korea University) ;
  • Kim, Woong (Department of Materials Science and Engineering, Korea University) ;
  • Kim, Jeong-Kwon (Department of Chemistry, Chungnam National University)
  • 발행 : 2010.01.20
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초록

A comprehensive comparative investigation of small carbohydrates in laser desorption ionization was performed on supporting materials composed of sodiated 2,5-dihydroxybenzoic acid (DHB), carbon nanotubes, an ionic liquid matrix of DHB-pyridine, a binary matrix of DHB-aminopyrazine, zinc oxide nanoparticles, and gold nanoparticles. The abundance of $[M+Na]^+$ ions, where M is glucose or sucrose, was compared for each supporting material. The highest sensitivity for both glucose and sucrose, with a detection limit of 3 pmol, was observed with carbon nanotubes. Both carbon nanotubes and the ionic liquid matrix exhibited the highest reproducibility.

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