The Characteristics of Acoustic Emission of $Al_2O_3$ Ceramics by an Amount of Additive $Y_2O_3$

소결조제 $Y_2O_3$ 함유량에 따른 $Al_2O_3$ 세라믹스의 음향방출 특성

  • Kim, Jin-Wook (Korea Institute of Materials Science) ;
  • Ahn, Seok-Hwan (School of Mechanical Engineering, Pukyong National University) ;
  • Nam, Ki-Woo (Division of Materials Science and Engineering, Pukyong National University)
  • Published : 2008.06.30

Abstract

This paper illustrates haw $Y_2O_3$ contributes to crack-healing strengths as a function of crack-healing temperature and the additive amount. In investigating mechanical properties, the indentation fracture method is very simple and useful, but careful attention must be paid to the statistical data processing because data may be scattered excessively, especially for brittle materials. To estimate accurate AE signal properties we applied the useful time-frequency method with a discrete wavelet analysis algorithm. In experiments, three kinds of specimens were prepared. After the specimens were indented by a Vickers indentor, they were heat-treated and crack-healed to evaluate bending strength and the AE signal. With higher amounts of the additive powder, as 1, 3, or 5% wt. of $Y_2O_3$, the concentrative tendency of dominant frequency trended toward lower frequency groups. The $Al_2O_3$ ceramic with 3% wt. of $Y_2O_3$ was judged most suitable because it demonstrated superior crack-healing ability and relative concentration on the highest frequency group.

Keywords

References

  1. 김진욱, 김해숙, 손창석, 안석환, 남기우 (2007). '$Al_{2}$$O_{3}$ 복합 세라믹스의 균열 진전에 따른 탄성파 특성', 2007년도 한국해양공학회 추계학술대회 논문집, pp 295-298
  2. 김해숙, 안석환, 손창석, 남기우 (2007). '$Y_{2}$$O_{3}$ 양에 따른 $Al_{2}$$O_{3}$ 복합 세라믹스의 고온 강도 특성', 2007년도 한국해양공학회 추계학술대회 논문집, pp 303-306
  3. 남기우, 김해숙, 손창석, 김성광, 안석환 (2007). '$Y_{2}$$O_{2}$ 첨가량에 의한 $Al_{2}$$O_{3}$ 복합재 세라믹스의 균열 치유와 고온 굽힘강도 특성', 대한기계학회논문집A, 제31권, 제11호, pp 1108-1114
  4. Ahn, S.H., Nam, K.W. and Ando, K. (2004). 'The Bending Strength of Brittle Materials and The Characteristics of the Elastic Wave Signal by Vickers Indentation', Key Engng. Mater., Vol 261-263, pp 1635-1640 https://doi.org/10.4028/www.scientific.net/KEM.261-263.1635
  5. Ando, K., Chu, M.C., Kobayashi, Y., Yao, F. and Sato, S. (1999). 'Crack Healing Behavior and High Temperature Strength of Silicon Nitride Ceramics', Jpn, Soc. Mech. Eng., Vol 65-633A, pp 1132-1139 (in Japanese)
  6. Ando, K., Shirai, Y., Nakatani, M., Kobayashi, Y. and Sato, S. (2002). '(Crack - healing + proof test): A New Methodology to Guarantee the Structural Integrity of a Ceramics Component', J. Eur. Ceram Soc., Vol 22, pp 121-128 https://doi.org/10.1016/S0955-2219(01)00236-9
  7. Ando, K., Kim, B.S., Chu, M.C., Saito, S. and Takahashi, K. (2004). 'Crack-healing and Mechanical Behaviour of $Al_{2}$$O_{3}$/SiC Composites at Elevated Temperature', Fatigue Fract Engng Mater Struct Vol 27, pp 533-541 https://doi.org/10.1111/j.1460-2695.2004.00785.x
  8. Kim, J.W., Park, B.W., Ahn, S.H. and Nam, K.W. (2005). 'Elastic Wave Signal Characteristics of SiC Ceramics with Crack Healing Ability by Wavelet Analysis', Key Engineering Materials, Vol 297-300, pp 2046-2051 https://doi.org/10.4028/www.scientific.net/KEM.297-300.2046
  9. Lange, J.J. and Radford, K.C. (1970). 'Healing of Surface Cracks in Polycrystalline $Al_{2}$$O_{3}$', J. Am. Ceram. Soc., Vol 53, pp 420-421 https://doi.org/10.1111/j.1151-2916.1970.tb12148.x
  10. Lee, S.K., Ishida, W., Lee, S.Y., Naill, K.W. and Ando, K. (2005). 'Crack-Healing Behavior and Resultant Strength Properties of Silicon Carbide Ceramic', J. Eur. Ceram. Soc., Vol 25, pp 569-576 https://doi.org/10.1016/j.jeurceramsoc.2004.01.021
  11. Nam, K.W., Kim, M.K., Kim, H.S., Kim, J.W. and Ahn, S.H. (2006). 'Bending Strength of Si3N4 Monolithic and Si3N4/SiC Composite Ceramics and Elastic Wave Characteristics by Wavelet Analysis', International Journal of Modem Physics B, Vol 20, No 25-27, pp 4279-4284 https://doi.org/10.1142/S0217979206041227
  12. Mistler, R.E. and Coble, R.L. (1971). 'Rate-determining Species in Diffusion-Controlled Processes in Al203', J. Am. Ceram. Soc., Vol 54, pp 60-61 https://doi.org/10.1111/j.1151-2916.1971.tb12175.x
  13. Zhao, J., Steams, L.C., Harmer, M.P., Chan, H.M. and Miller, G.A. (1991). 'Mechanical Behavior of Alumina-silicon Nonocomposites', J. Am. Ceram. Soc., Vol 76, pp 503-510 https://doi.org/10.1111/j.1151-2916.1993.tb03814.x
  14. Newland, D.E. (1993). An Introduction to Random Vibrations, Spectral and Wavelet Analysis, Wiley, pp 348-353