GC-MS Analysis of Volatile Constituents from Acanthopanax sessiliflorus

오갈피나무의 정유성분 GC-MS 분석

  • Lim, Soon-Sung (Department of Food Science and Nutrition, Hallym University) ;
  • Lee, Yeon-Sil (Department of Food Science and Nutrition, Hallym University) ;
  • Lee, Sul-Lim (Department of Applied Plant Science, Chung-Ang University) ;
  • Kim, Jong-Kee (Department of Applied Plant Science, Chung-Ang University) ;
  • Cho, Seon-Haeng (Gongju National University of Education) ;
  • Shin, Kuk-Hyun (Korea Institute of Science and Technology Information) ;
  • Lee, Sang-Hyun (Department of Applied Plant Science, Chung-Ang University)
  • 임순성 (한림대학교 식품영양학과) ;
  • 이연실 (한림대학교 식품영양학과) ;
  • 이설림 (중앙대학교 식물응용과학과) ;
  • 김종기 (중앙대학교 식물응용과학과) ;
  • 조선행 (공주교육대학교) ;
  • 신국현 (한국과학기술정보연구원) ;
  • 이상현 (중앙대학교 식물응용과학과)
  • Published : 2008.03.31

Abstract

The chemical composition of the volatile constituents from the leaves, stems, and roots of Acanthopanax sessiliforus growing wild in Mt. Deok-Yu was determined by GC and GC-MS spectrometric analysis with the aid of NBS, Wiley Library and RI indice searches. The major constituents identified were ${\delta}-3-carene$ (7.24%), limonene (8.10%), ${\beta}-thujene$ (17.85%), trans-bicyclic hydrocarbon (13.35%) and ${\delta}-cadinene$ (4.28%) in the leaves from one year-grown plants, tricyclene (7.21%), ${\beta}-myrcene$ (7.62%), limonene (10.23%), ${\beta}-thujene$ (15.61%) and dihydroedulan I (6.12%) in the leaves from three years-grown plants, ${\delta}-3-carene$ (4.96%), limonene (5.93%), ${\beta}-phellandrene$ (17.31%) and naphthalene (7.79%) in the stems from one year-grown plants, ${\alpha}-pinene$ (5.21%), limonene (5.12%) and ${\beta}-phellandrene$ (9.82%) in the stems from three years-grown plants, ${\alpha}-pinene$ (12.73%), ${\beta}-pinene$ (11.16%), ${\delta}-3-carene$ (6.16%) and ${\gamma}-cadinene$ (23.39%) in the roots from one year-grown plants, and ${\alpha}-pinene$ (17.25%), ${\beta}-pinene$ (9.35%), ${\delta}-3-carene$ (7.26%) and ${\gamma}-cadinene$ (17.95%) in the roots from three years-grown plants.

Keywords

References

  1. Yook, C. S. (1999) Colored Medicinal Plants of Korea, 372. Academy Publishing Co., Korea
  2. Jun, W. J., Seong, H. S., Chun, H., Lim, E. J., Kim, K. I. and Cho, H. Y. (2007) Determination of antioxidative potentials of Acanthopanax sessiliflorus (Rupr. & Maxim.) Seem. in differentiated HL-60 cells. Food Chem. 105: 1557-1563 https://doi.org/10.1016/j.foodchem.2007.01.056
  3. Lee, P., Lee, S., Choi, S. Y. and Son, D. (2005) Neuroprotective effect of Acanthopanax sessiliflorus against toxicity induced by N-methyl-D-aspartate in rat organotypic hippocampal slice culture. Nat. Prod. Sci. 11: 179-182
  4. Chung, K. C., Baek, S. H. and Nam, K. S. (1988) Studies on the antimutagenic effect of Acanthopanax sessiliflorum components. Yakhak Hoeji 32: 14-19
  5. Ryoo, H. S., Park, S. Y., Chang, S. Y. and Yook, C. S. (2003) Triterpene components from the leaves of Acanthopanax sessiliflorus Seem. Kor. J. Pharmacogn. 34: 269-273
  6. Lee, S., Kim, B.-K., Cho, S. H. and Shin, K. H. (2002) Phytochemical constituents from the fruits of Acanthopanax sessiliflorus. Arch. Pharm. Res. 25: 280-284 https://doi.org/10.1007/BF02976626
  7. Kim, C. W. and Kim, S. K. (1987) Studies on the constituents of seeds of Acanthopanax sessiliflorum Seemann (I). On fatty acids and sterols. Kor. J. Pharmacogn. 18: 184-187
  8. Yook, C. S., Lee, D. H., Seo, Y. K. and Ryu, K. S. (1977) Study on the constituents in the root bark of Acanthopanax sessiliflorum Seemann (11). Kor. J. Pharmacogn. 8: 31-34
  9. Lee, S., Chung, H. S., Shin, K. H. and Kim, B.-K. (2004) Determination of hyperin in Acanthopanax senticosus and A. sessiliflorus by HPLC. Yakhak Hoeji 48: 231-235
  10. Lim, S. S., Lee, J. M., Park, H. S., Cho, S. H., Shin, K. H. and Lee, S. (2007) GC-MS analysis of volatile constituents from Acanthopanax senticosus. Kor. J. Pharmacogn. 38: 327-333
  11. Egon, S. (1973) Thin-Layer Chromatography, 2nd Ed., George Allen & Unwin, 208. Springer-Verlag
  12. McLafferty, F. W. and Stauffer, D. B. (1989) The Wiley/NBS Registry of Mass Spectral Data
  13. Wagner, H., Bladt, S. and Zgainski, E. M. (1984) Plant Drug Analysis, Springer-Verlag