DOI QR코드

DOI QR Code

MICROSTRUCTURAL EVOLUTION OF A HIGH CR FE-BASED ODS ALLOY BY DIFFERENT COOLING RATES

  • Shen, Yin-Zhong (Nuclear Materials Research Center, Korea Atomic Energy Research Institute) ;
  • Cho, Hae-Dong (Nuclear Materials Research Center, Korea Atomic Energy Research Institute) ;
  • Jang, Jin-Sung (Nuclear Materials Research Center, Korea Atomic Energy Research Institute)
  • Published : 2008.03.31

Abstract

Through mechanical alloying, hot isostatic pressing and hot rolling, a 9%Cr Fe-based oxide dispersion-strengthened alloy sample was fabricated. The tensile strength of the alloy is significantly improved when the microstructure is modified during the post-consolidation process. The alloy samples were strengthened as the cooling rates increased, though the elongation was somewhat reduced. With a cooling rate of $800^{\circ}C/s$ after normalization at $1150^{\circ}C$, the alloy sample showed a tensile strength of 1450 MPa, which is about twice that of the hot rolled sample; however, at $600^{\circ}C$ the tensile strength dramatically decreased to 620 MPa. Optical microscope and transmission electron microscope were used to investigate the microstructural changes of the specimens. The resultant strengthening of the alloy sample could be mainly attributed to the interstitially dissolved nitrogen, the fraction of the tempered martensite, the fine grain and the presence of a smaller precipitate. The decrease in the tensile strength was mainly caused by the precipitation of vanadium-rich nitride.

Keywords

References

  1. R. Schaublin, A. Ramar, N. Baluc, V. de Castro, M. A. Monge, T. Leguey, N. Schmid and C. Bonjour, 'Microstructural Development under Irradiation in European ODS Ferritic /Martensitic Steels,'J. Nucl. Mater. 351, 247 (2006) https://doi.org/10.1016/j.jnucmat.2006.02.005
  2. R. L. Klueh, P. J. Mashimoto, I. S. Kim, L. Heatherly, D. T. Hoelzer, N. Hashimoto, E. A. Kenik and K. Miyahara, 'Tensile and Creep Properties of an Oxide Dispersionstrengthened Ferritic Steel,' J. Nucl. Mater. 307-311, 773 (2002) https://doi.org/10.1016/S0022-3115(02)01046-2
  3. C. Cayron, E. Rath, I. Chu and S. Launois, 'Microstructural Evolution of Y2O3 and $MgAl_2O_4$ ODS EUROFER Steels during their Elaboration by Mechanical Milling and Hot Isostatic Pressing,' J. Nucl. Mater. 333, 83 (2004)
  4. H. Sakasegawa, S, Ohtsuka, S. Ukai, H,Tanigawa, M.Fujiwara, H. Ogiwara and A. Kohyama, 'Microstructual Evolution during Creep of 9Cr-ODS Steels,' Fusion Engineering and design 81, 1013 (2006) https://doi.org/10.1016/j.fusengdes.2005.09.045
  5. T. Shibayama, I. Yamagata, H. Kurishita and H. Kayano, 'Development of oxide dispersion strengthened vanadium alloy and its properties,' J. Nucl. Mater. 239, 162 (1996) https://doi.org/10.1016/S0022-3115(96)00469-2
  6. M. L. G. Byrnes, M. Grujicic and W. S. Owen, 'Nitrogen strengthening of a stable austenitic stainless steel,' Acta Metall., 35, 1853 (1987) https://doi.org/10.1016/0001-6160(87)90131-3
  7. E. Werner, 'Solid solution and grain size hardening of nitrogen-alloyed austenitic steels,' Mater Sci Eng , A101, 93 (1988)
  8. H. A. Wriedt, N. A. Gokcen and R. H. Nafziger: Binary Alloy Phase Diagrams, 2nd ed., by T. B. Massalski, H. Okamoto, P. R. Subramanian and L. Kacprzak, ASM, Metals Park, Ohio, 1729 (1990)