Stability and Processing Characteristics of Microencapsulated Squid Liver Oil by Fluidized Bed Coating

오징어 간유 미세캡슐의 유동층 코팅에 따른 품질 특성

  • Hwang, Sung-Hee (Department of Food Science and Technology, Catholic University of Daegu) ;
  • Youn, Kwang-Sup (Department of Food Science and Technology, Catholic University of Daegu)
  • 황성희 (대구가톨릭대학교 외식식품산업학부) ;
  • 윤광섭 (대구가톨릭대학교 외식식품산업학부)
  • Published : 2008.12.31

Abstract

Squid oil is an abundant source of polyunsaturated fatty acids. This is particularly true for eicosapentaenoic acid and docosahexaenoic acid. The principal objective of this study was to extend the stability and improve the process aptitude of squid liver oil. Fluidized bed coatings were employed for coating with microencapsulated oil. The efficiency of the fluidized bed coating of the microencapsulated powder was over 90%. The apparent density with zein-DP was 0.6 g/mL, thereby indicating that flow ability had been improved as the result of an increase in specific gravity. The solubility of artificial gastric and enteric fluids with HPMC-FCC was 59.9 and 0%, respectively, whereas with zein-DP solubility was 0 and 31.0%, respectively. Polyunsaturated fatty acid retention results demonstrated that zein-DP coating was higher than HPMC-FCC, followed by the microencapsulated squid liver oil method. These results demonstrated that the application of microencapsulation and fluidized bed micro-coating techniques improved the stability and processing compatibility of squid liver oil.

오징어 간유 미세캡슐화 분말을 HPMC-FCC, zein-DP로 코팅하여 유동층 코팅 특성을 살펴본 결과, 유동층 코팅 효율은 HPMC-FCC, zein-DP 모두 90%의 효율을 나타내었다. 겉보기 밀도는 zein-DP 코팅분말이 0.6 g/mL로 높게 나타나 코팅 분말의 비중이 커져 흐름성이 개선되었음을 확인할 수 있었다. 인공위액과 인공장액에 대한 용해성을 살펴본 결과, HPMC-FCC는 각각 59.9%와 0%를 나타내었고 zein-DP는 각각 0%와 31.0%를 나타내어 코팅재료에 따라 용해성을 조절할 수 있었다. 저장 안정성은 zein-DP나 HPMC-FCC로 코팅한 분말이 미세캡슐화 분말보다 높은 PUFA/SFA 잔존율을 보여, 유동층 코팅 기술이 유지식품의 안정성을 확보할 수 있는 새로운 기술이 될 수 있음을 확인할 수 있었다.

Keywords

References

  1. Michijiou Suyama, Shouji Kounosu, Mototsugu Hamabe, Yukio Okuda. Utilization of squid. Kouseisha kouseikaku. Tokyo. pp. 52-100 (1983)
  2. Yi YS, Kang HH, Chang KS, Chang YI. Effect of some anticaking conditioners on the flowability of dried garlic powder. Korean J. Food Sci. Technol. 30: 1357-1361 (1998)
  3. Dewettinck K, Messens W, Deroo L, Huyghebaert A. Agglomeration tendency during top-spray fluidized bed coating with gelatin and starch hydrolysate. Lebensm-Wisse. Technol. 32: 102-106 (1999) https://doi.org/10.1006/fstl.1998.0507
  4. Malamataris S, Karidas T, Goidas P. Effect of particle size and sorbed moiture on the compression behavior of some hydroxypropyl methylcellulose(HPMC) polymer. Int. J. Pharm. 103: 205-215 (1994) https://doi.org/10.1016/0378-5173(94)90170-8
  5. Cheong LWS, Heng PWS, Wong LF. Relationship between polymer viscosity and drug release from a matrix system. Pharm. Res. 9: 1510-1514 (1992) https://doi.org/10.1023/A:1015883501871
  6. Kim YH, Kim DM, Kim KH. Permeability and mechanical properties of zein and gluten-based films. Korean J. Food Sci. Technol. 26: 138-140 (1994)
  7. Mose AJ. Gastroretentive dosage forms. Crit. Rev. Ther. Drug 10: 143-195 (1993)
  8. Seo JY, Shin MG. Analysis of microencapsulation yield of sardine oil spray drying. J. Korean Soc. Food Sci. Nutr. 28: 274-276 (1999)
  9. The Korean Pharmacopoeia VIII. Korean Pharmacy College Council. Pharmacopoeia Subcommittee. ShinIl books, Seoul. pp. 1636-1640 (2003)
  10. Song JY, Kim YC, Shin MS. Textural properties and structures of wheat and maize starch-gum mixed gels during storage. Food Sci. Biotechnol. 17: 20-25 (2008)
  11. AOCS. Official Methods and Recommended Practeces of the American Oil Chemists' Society. Cd 12-57. $4^{th}$ ed. American Oil Chem. Soc. Champaign, IL, USA (1990)
  12. Minoru Y, Kenji H. Fatty acid composition of lipids from 22 species of fish and mollusk. Bull. Jpn Soc. Sci. Fish. 41: 1143-1152 (1975) https://doi.org/10.2331/suisan.41.1143
  13. Kang HA, Shin MG. Effect of inlet air temperature and atomizing pressure on fluidizedbed coating efficiency of broken peanut. Korean J. Food Sci. Technol. 34: 924-926 (2002)