Microstructure of Titania Layers Formed by Plasma Electrolytic Oxidation (PEO) Method

  • Ok, Myoung-Ryul (Materials Science and Technology Division, Korea Institute of Science and Technology) ;
  • Kim, Ji Hye (Materials Science and Technology Division, Korea Institute of Science and Technology) ;
  • Kang, Eun Young (Materials Science and Technology Division, Korea Institute of Science and Technology) ;
  • Hong, Kyung Tae (Materials Science and Technology Division, Korea Institute of Science and Technology)
  • Published : 2006.12.01

Abstract

Titania coatings were prepared on commercially pure Ti by plasma electrolytic oxidation (PEO) method with various electrolytes and process condition. Coatings were formed under galvanostatic condition with several current density values, and the change of applied voltage with process time was recorded. The microstructure of the titania coatings was observed using XRD, SEM, TEM, and the time-voltage diagrams were analyzed in terms of microstructure evolution.

Keywords

References

  1. A. L. Yerokhin, X. Nie, A. Leyland, and A. Mathews, Surf. Coat. Tech., 122, 73 (1999) https://doi.org/10.1016/S0257-8972(99)00441-7
  2. X. Nie, A. Leyland, A. Mathews, J. C. Jiang, and E. I. Meletis, J. Biomed. Mater. Res., 57, 612 (2001) https://doi.org/10.1002/1097-4636(20011215)57:4<612::AID-JBM1208>3.0.CO;2-H
  3. A. L. Yerokhin, A. Shatrov, V. Samsonov, P. Shashkov, A. Leyland, and A. Mathews, Surf Coat. Tech., 182, 78 (2004) https://doi.org/10.1016/S0257-8972(03)00877-6
  4. O. P. Terleeva, Y-J. Oh, M.-R. Ok, V. V. Utkin, H.-P. Ha, and D.-H. Lee, Mater. Trans. JIM, 4, 2467 (2005)
  5. Yong Han, Seong-Hyeon Hong, and Kewei Xu, Surf Coat. Tech., 168, 249 (2003) https://doi.org/10.1016/S0257-8972(03)00016-1
  6. J. Schreckenbach, F. Schlottig, and G. Marx, J. Mater.Res., 14, 1437 (1999) https://doi.org/10.1557/JMR.1999.0194
  7. H. Guo, M. An, S. Xu, and H. Huo, Mater. Lett., 60, 1538 (2006) https://doi.org/10.1016/j.matlet.2005.11.066
  8. M. Boinet, S. Verdier, S. Maximovitch, and F. Dalard, Surf. Coat. Tech., 199, 141 (2005) https://doi.org/10.1016/j.surfcoat.2004.10.145
  9. V. Zwilling, M. Aucouturier, and E. Darque-Ceretti, Electrochimica Acta, 45, 921 (1999) https://doi.org/10.1016/S0013-4686(99)00283-2
  10. X. Sun, Z. Jiang, S. Xin, and Z. Yao, Thin Solid Film, 471, 194 (2005) https://doi.org/10.1016/j.tsf.2004.06.096
  11. T. J. Webster, R. W. Siegel,and R. Bizions, Biomaterials, 21, 1803 (2000). https://doi.org/10.1016/S0142-9612(00)00075-2
  12. L. O. Snizhko, A. L. Yerokhin, A. Pilkington, and N. L. Gurevina, Electrochimica Acta, 49, 2085 (2004) https://doi.org/10.1016/j.electacta.2003.11.027
  13. H. Habazaki, M. Uozumi, H. Konno, K. Shimizu, P. Skeldon, and G. E. Thompson, Corrosiom Sci., 45, 2063 (2003) https://doi.org/10.1016/S0010-938X(03)00040-4