Microstructure Effects on Bending Strength Characteristics of LPS - SiC Ceramic

LPS - SiC 세라믹스의 굽힘강도 특성에 미치는 미시조직 영향

  • Yoon, Han-Ki (Department of Mechanical Engineering, Dongeui University) ;
  • Jung, Hun-Chae (Graduate School of Mechanical Engineering, Dongeui University)
  • 윤한기 (동의대학교 기계공학과) ;
  • 정헌채 (동의대학교 대학원 기계공학과)
  • Published : 2006.10.31

Abstract

In this study, monolithic liquid phase sintered SiC (LPS-SiC) was made by the hot pressing method with nano-SiC powder, whose particle size is 30 nm and less on the average. Alumina ($Al_{2}O_{3}$), yttria ($Y_{2}O_{3}$), and silica ($S_{i}O_{2}$) were used for sintering additives. To investigate the effects of $S_{i}O_{2}$, the $Al_{2}O_{3}/Y_{2}O_{3}$ composition was fixed and the ratio of $S_{i}O_{2}$ was changed, with seven different ratios tested. And to investigate the effects of the sintering temperature, the sintering temperature was changed, with $1760^{\circ}C,\;1780_{\circ}C$, and $1800_{\circ}C$ being used with a $S_{i}O_{2}$ ratio of 3 wt%. The materials were sintered for 1 hour at $1760^{\circ}C,\;1780^{\circ}C$ and $1800^{\circ}C$ under a pressure of 20 MPa. The effects on sintering from the sintering system used, as well as from the composition of the sintering additives, were investigated by density measurements. Mechanical properties, such as flexural strength, were investigated to ensure the optimum conditions for a matrix of SiCf/SiC composites. Sintered densityand the flexural strength of fabricated LPS-SiC increased with an increase in sintering temperature. Particularly, the relative density of a sintered body at $1800^{\circ}C$ with a non-content of $S_{i}O_{2}$, a specimen of AYSO-1800, was 95%. Also, flexural strength was about 750MPa.

Keywords

References

  1. Hasegawa, A., Kohyama, A., Jones, R.H., Snead, L.L., Riccardi. B. and Fenici, P. (2000). 'Critical issues and current status of SiC/SiC composites for fusion,' Journal of Nuclear Materials, Vol283-287, pp 128-137 https://doi.org/10.1016/S0022-3115(00)00374-3
  2. Lee, S.P., Yoon, H.K., Park, J.S., Katoh, Y., Kohyama, A., Kim, D.H. and Lee, J.K. (2002). 'Reaction Sintering Process of Tyranno SA/SiC Composites and their Characterization', Fusion Engineering and Design, Vol 61-62, pp 717-722 https://doi.org/10.1016/S0920-3796(02)00151-5
  3. Ohring, M. (1995). 'Engineering Materials Science', ACADEMIC PRESS, ISBN 0-12-524995-0
  4. Padture, N.P. and lawn, B.R. (1994). 'Toughness Properties of a Silicon Carbide with and in Situ Induced Heterogeneous Grain Structure', Journal of American Ceramic Society, Vol 77, No 10, pp 853-859
  5. Park, Y.H., Yoon, H.K., Lee, G.G., Lee, J.G., Katoh, Y. and Kohyama, A. (2003). 'Fabrication and High Temperature Flexural Strength Properties of Monolithic SiC Fabricated by Liquid-Phase Sintering Method', Proceedings of the KSME Busan Branch 2003 Springtime Annual Meeting, pp 59-63
  6. Raffray, A.R., Jones, R., Aiello, G., Billone, M., Giancarli, L., Golfier, H., Hasegawa, A., Katoh, Y., Kohyama, A., Nishio, S., Riccardi, B. and Tillack, M.S. (2001). 'Design and material issues for high performance SiCf/SiC-based fusion power cores,' Fusion Engineering and Design, Vol 55, pp 55-95 https://doi.org/10.1016/S0920-3796(01)00181-8
  7. Snead, L.L., Jones, R.H., Kohyama, A. and Fenici, P. (1996). 'Status of silicon carbide composites for fusion', Journal of Nuclear Materials, Vol 233-237, pp 26-36 https://doi.org/10.1016/S0022-3115(96)00318-2