KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY (한국포장학회지)

Korea Society of Packaging Science and Technology (한국포장학회)
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Synthesis and Characterization of Titanoalumino Silicalite

티타노알루미노 실리카라이트의 합성 및 특성연구

  • Ko, Yong-Sig (Dept. of Advanced Material Chemistry, Shinsung College) ;
  • Kim, Sang-Min (Dept. of Advanced Material Chemistry, Shinsung College)
  • 고용식 (신성대학 신소재화학과) ;
  • 김상민 (신성대학 신소재화학과)
  • Published : 2005.06.30
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Abstract

Titanoalumino silicalite (TAS) was prepared hydrothermally, and the effects of synthesis parameters such as silica/alumina sources, $SiO_2/TiO_2$ ratio, and aging treatment were investigated. The structure, crystal size, and shape were examined by XRD and SEM, and the extent of titanium incorporation into the zeolite framework was examined using UV-vis DRS spectroscopy. For TAS preparation, aging of ca. 24h was essential, and the faster crystallization rates were achieved with Cab-O-Sil than with Ludox or TEOS as a silica source. In addition, the higher crystallinity and faster crystallization rate were obtained using sodium aluminate as an aluminum source.

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