A Study on Synthesis of Functional Composite Latex and Characteristics of Thermal Decomposition

기능성 복합 라텍스의 합성과 열분해 특성에 관한 연구

  • Kwon, Jae-Beom (Department of Safety Engineering, Pukyong National University) ;
  • Kim, Nam-Suk (Department of Safety Engineering, Pukyong National University) ;
  • Lee, Nae-Woo (Department of Safety Engineering, Pukyong National University) ;
  • Seul, Soo-Duck (Department of Chemical Engineering, Dong-A University)
  • 권재범 (부경대학교 안전공학과) ;
  • 김남석 (부경대학교 안전공학과) ;
  • 이내우 (부경대학교 안전공학과) ;
  • 설수덕 (동아대학교 화학공학과)
  • Published : 2004.06.01

Abstract

Emulsion polymerization ws carried out using Alkyl methacrylate(RMA) like MMA, EMA, BMA and Styrene Monomer(SM) for core-shell latex preparation. It was synthesized at $80^{\circ}C$ in the presence of anionic surfactant SLS(Sodium Lauryl Sulfate). FT-IR and DSC analysis are used to confirm the synthesized core-shell emulsion latexes. Moreover DSC and TGA were used to investigate the thermal characterisitcs of them. The differences of the decomposition rate and the activation energy from TGA and DSC analysis are not so big. It considers that the pendent group is not affect of the thermal characteristics and stability on core-shell latexes, which is synthesized with RMA and Styrene. For investigating combustion products, LC50 values were calculated by FED(Fractional Effective Dose)from the Pyrolyzer-Mass sepctrometer.

Keywords

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