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Determination of the Mechanical Properties of the Coated Layer in the Sheet Metal Using Load-Displacement Curve by Nanoindentation Technique

나노 인덴테이션의 하중-변위 곡선을 이용한 용융아연도금 강판 코팅층의 기계적 특성 결정

  • 고영호 (부산대학교 정밀기계공학과) ;
  • 이정민 (부산대학교 정밀기계공학과) ;
  • 김병민 (부산대학교 정밀정형 및 금형가공연구소)
  • Published : 2004.12.01

Abstract

Mechanical properties such as Young's modulus and hardness of thin film in coated steel are difficult to determine by nano-indentation from the conventional analysis using the load-displacement curve. Therefore, an analysis of the nano-indentation loading-unloading curve was used to determine the Young's modulus, hardness. A new method is recently being developed for elastic-plastic properties of materials from nano-indentation. Elastic modulus of the thin films shows relatively small influence whereas yield strength is found to have significant effect on measured data. The load-displacement curves of material tested with a Berkovich indenter and nano-indentation continuous stiffness method is used to measure the modulus and hardness through thin films, and then these are computed using the analysis procedure. The developed neural networks apply also to obtain reliable mechanical properties.

Keywords

References

  1. William D. Nix, 1997, 'Elastic and plastic properties of thin films on substrates: nanoindentation techni-ques', Mat. Sci and Eng , A234-236, pp37-44
  2. D. H. Shin, 2001, 'Plastic flow characteristics of ultrafine grained low carbon steel during tensile deformation', Metals and Meterials Int. Vol.7, No. 6, pp.573-577 https://doi.org/10.1007/BF03179256
  3. H. Pelletier, J. Krier, A. Cornet, P. Mille, 2000, 'Limits of using bilinear stress-strain curve for finite element modeling for nanoindentation response on bulk.', Thin Solid Films, Vol.379, pp.147-155 https://doi.org/10.1016/S0040-6090(00)01559-5
  4. S. Chowdhury, M. T. Laugier, I. Z. Rahman , 2003, 'Measurement of the mechanical properties of carbon nitride thin films from the nanoindentation loading curve', Diamond and Related Materials
  5. Anthony. C. Fisher-Cripper, 'Nanoindentation'
  6. Sheddon, 'The relation between load and penetration in the axisymmetric boussing problem for a punch of arbitrary profile' Int, J, Eng, Sci, Vol3, pp.47-57
  7. L. Gan, B.Ben-Nissan, 1997, 'The effects of mecha-nical properties of thin films on nanoindentation data : Finite element analysis', Com. Mat. Sci. Vol8, pp.273-278 https://doi.org/10.1016/S0927-0256(97)00040-2
  8. J. A. Knapp, D. M. Follstaedt, J. C. Barbour, S. M. Myers, 'Finite-element modeling of nanoindentation for determining the mechanical properties of imp-lanted layer and thin films' NIMB Vol 127/128, pp.935-939 https://doi.org/10.1016/S0168-583X(97)00034-7
  9. H. Elghazal, G. Lormand, A.Hamel, D.Girodin, A. Vincent 'Microplasticity characteristics obtained through nano-indentatin measurements: application to surface hardness steels' Mat. Sci and Eng, A303, pp. 110-119
  10. Yo-Han Yoo, Woong Lee, Hyunho Shin 'Effect of work hardening on the critical indentation limit in spherical nano-indentation of thin film/substrate systems', Surface and Coating Technology. 179, pp. 324-332
  11. Ranjana Saha, Zhenyu Xue, Young Huang, William D. Nix, 'Indentation of a soft metal film on a hard substrature: strain gradient hardening effects', J. M. P. S, 49, pp. 1997-2014
  12. 이정우, 윤성원, 강충길, '나노 인덴테이션 공정의 유한요소해석 및 실험적 검증', 한국소성가공학회지, Vol.12, No.4, pp.382-387
  13. Dejun Ma, Kewei Xu, Jiawen He, Jian Lu 'Evaluation of the mechanical properties of thin metal films', Surface and Coating Technology, 116 -119, pp. 128-132 https://doi.org/10.1016/S0257-8972(99)00218-2