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Sintering Behavior of (Ti+Ni) Powder Mixture during Spark-Plasma Sintering

방전플라즈마소결에 있어서의 (Ti+Ni) 혼합불말의 소결거동

  • 김지순 (울산대학교 첨단소재공학부, 기계부품및소재특성평가연구센터(ReMM)) ;
  • 양석균 (울산대학교 첨단소재공학부, 기계부품및소재특성평가연구센터(ReMM)) ;
  • 정순호 (울산대학교 첨단소재공학부, 기계부품및소재특성평가연구센터(ReMM)) ;
  • 강지훈 ((주)바이오스마트) ;
  • 권영순 (울산대학교 첨단소재공학부, 기계부품및소재특성평가연구센터(ReMM))
  • Published : 2004.02.01

Abstract

TiNi bodies were produced from (Ti+Ni) powder mixture by spark-plasma sintering procerg. The sintering behavior was investigated through the measurement of change in density, densification rate, phase analysis and microstructure. Irrespective of heating rate, sintered bodies with above 97% relative density could be obtained. TiNi with B2 structure was confirmed as the major phase and $Ti_2Ni,\;TiNi_3$, unreacted Ti, Ni as the second phase. Increase in heating rate suppressed a formation of intermediate phase during sintering process. Increase in holding time at sintering temperature led to a compositional homogenization.

Keywords

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