DOI QR코드

DOI QR Code

2,4,6-Triamino-1,3,5-triazin-1-ium Acetate Acetic Acid Solvate Monohydrate. Infrared and Raman Spectra

  • Marchewka, M.K. (Institute of Low Temperature and Structure Research, Polish Academy of Sciences)
  • Published : 2004.04.20

Abstract

The crystals of the new melaminium salt, i.e. melaminium acetate acetic acid solvate monohydrate, $C_3H_7N_6^+ {\cdot}CH_3COO^- {\cdot}CH_3COOH{\cdot}H_2O$, were obtained by the slow evaporation of an aqueous solution at room temperature. Powder infrared and Raman spectra were measured and interpreted. The vibrational spectra in the region of internal vibrations of ions corroborate structural data recently published by Perpetuo and Janczak.$^1$ Some spectral features of this new crystal are referred to corresponding one for melamine crystal as well as other melamine complexes in crystalline form. Hydrogen-bonded network present in the crystal gives notable vibrational effect.

Keywords

References

  1. Perpetuo, G. J.; Janczak, J. Acta Cryst. 2002, C58, o112.
  2. Kakihana, M.; Kotaka, M.; Okamoto, M. J. Phys. Chem. 1982, 86,4385. https://doi.org/10.1021/j100219a022
  3. George, W. O.; Houston, T. E.; Harris, W. C. Spectrochim. Acta1974, 30A, 1035.
  4. Kim, S. B.; Hammaker, R. M.; Fateley, W. G. Spectrochim. Acta1985, 41A, 167.
  5. Kim, S. B.; Hammaker, R. M.; Fateley, W. G. Spectrochim. Acta1985, 40B, 1295.
  6. Raso, M. A.; Garcia, M. V.; Morcillo, J. J. Mol. Struct. 1984, 115,449. https://doi.org/10.1016/0022-2860(84)80109-X
  7. Maes, G. Spectroscopy Letters 1983, 16, 311. https://doi.org/10.1080/00387018308062348
  8. Ha, T.-K.; Paul, C.; Ghosh, P. N. Spectrochim. Acta 1992, 48A,1083.
  9. Matzke, P.; Chacon, O.; Andrade, C. J. Mol. Struct. 1971, 9, 255. https://doi.org/10.1016/0022-2860(71)85042-1
  10. Koleva, V.; Stoilova, D. J. Mol. Struct. 2002, 611, 1. https://doi.org/10.1016/S0022-2860(01)00957-7
  11. Zieba-Palus, J. J. Mol. Struct. 1999, 511-512, 327.
  12. Marchewka, M. K.; Ratajczak, H. Bull. Pol. Acad. Sci. Chem.2002, 3, 335.
  13. Zerkowski, J. A.; McDonald, J. C.; Whitesides, G. M. Chem.Mater. 1994, 6, 1250. https://doi.org/10.1021/cm00044a024
  14. Zerkowski, J. A.; Whitesides, G. M. J. Am. Chem. Soc. 1994, 116,4298. https://doi.org/10.1021/ja00089a019
  15. Janczak, J.; Perpétuo, G. J. Acta Cryst. 2001, C57, 1431.
  16. Janczak, J.; Perpétuo, G. J. Acta Cryst. 2001, C57, 123.
  17. Janczak, J.; Perpétuo, G. J. Acta Cryst. 2001, C57, 873.
  18. Janczak, J.; Perpétuo, G. J. Acta Cryst. 2001, C57, 1120.
  19. Tanbug, R.; Kirschbaum, K.; Pinkerton, A. J. Chem. Crystallogr.1999, 29, 45. https://doi.org/10.1023/A:1009519230690
  20. Martin, A.; Pinkerton, A. Acta Cryst. 1995, C51, 2174.
  21. Wang, Y.; Wei, B.; Wang, Q. J. Crystallogr. Spectr. Res. 1990, 20,79. https://doi.org/10.1007/BF01181678
  22. Scoponi, M.; Polo, E.; Pradella, F.; Bertolasi, V.; Carassiti, V.;Goberti, P. J. Chem. Soc. Perkin Trans. 2 1992, 1127.
  23. Kawasaki, T.; Kuroda, Y.; Nishikawa, H. J. Ceram. Soc. Jap.1996, 104, 935. https://doi.org/10.2109/jcersj.104.935
  24. Braga, D.; Angeloni, A.; Tagliavini, E.; Grepioni, F. J. Chem. Soc.,Dalton Trans. 1998, 12, 1961.
  25. Weber, E.; Dorpinghaus, N.; Wimmer, C.; Stein, Z.; Krupitsky, H.;Goldberg, I. J. Org. Chem. 1992, 57, 6825. https://doi.org/10.1021/jo00051a029
  26. Guru Row, T. N. Coordination Chem. Rev. 1999, 183, 81. https://doi.org/10.1016/S0010-8545(98)00184-2
  27. Aakeroy, C. B. Acta Cryst. 1979, B53, 569.
  28. Janczak, J.; Perpétuo, G. J. Acta Crystallogr. 2001, C57, 1.
  29. Meier, R. J.; Tiller, A.; Vanhommerig, S. A. M. J. Phys. Chem.1995, 99, 5457. https://doi.org/10.1021/j100015a031
  30. Jones, W. J.; Orville-Thomas, W. J. Trans. Faraday Soc. 1959, 55,203. https://doi.org/10.1039/tf9595500203
  31. Larkin, P. J.; Makowski, M. P.; Colthup, N. B.; Food, L. A.Vibrational Spectroscopy 1998, 17, 53. https://doi.org/10.1016/S0924-2031(98)00015-0
  32. Meier, R. J.; Maple, J. R.; Hwang, M. J.; Hagler, A. T. J. Phys.Chem. 1995, 99, 5445. https://doi.org/10.1021/j100015a030
  33. Schneider, J. R.; Schrader, B. J. Mol. Struct. 1975, 29, 1. https://doi.org/10.1016/0022-2860(75)88001-X
  34. Larkin, P. J.; Makowski, M. P.; Colthoup, N. B. Spectrochim. Acta1999, A55, 1011.
  35. Heyns, A. M. J. Mol. Struct. 1972, 11, 93. https://doi.org/10.1016/0022-2860(72)85223-2
  36. Novak, A. Structure and Bonding 1974, 18, 177. https://doi.org/10.1007/BFb0116438
  37. Wang, Y.-L.; Mebel, A. M.; Wu, C.-J.; Chen, Y.-T.; Lin, C.-E.;Jiang, J.-C. J. Chem. Soc. Faraday Trans. 1997, 93, 3445. https://doi.org/10.1039/a701732d
  38. Marchewka, M. K. Mat. Sci. Eng. 2002, B95, 214.
  39. Fernandez-Liencres, M. P.; Navarro, A.; Lopez-Gonzalez, J. J.;Fernandez-Gomez, M.; Tomkinson, J.; Kearley, G. J. Chem. Phys.2001, 266, 1. https://doi.org/10.1016/S0301-0104(01)00326-3
  40. Janczak, J.; Perpétuo, G. J. Acta Cryst. 2002, C58, o339.
  41. Perpetuo, G. J.; Janczak, J. Acta Cryst. 2002, C58, o431.
  42. Janczak, J.; Perpétuo, G. J. Acta Cryst. 2002, C58, o455.
  43. Marchewka, M. K. Mat. Lett. 2003, 58, 843. https://doi.org/10.1016/j.matlet.2003.07.022
  44. Marchewka, M. K.; Baran, J.; Pietraszko, A.; Haznar, A.; Debrus,S.; Ratajczak, H. Solid State Sci. 2003, 5, 509. https://doi.org/10.1016/S1293-2558(03)00029-3
  45. Marchewka, M. K.; Janczak, J.; Debrus, S.; Baran, J.; Ratajczak,H. Solid State Sci. 2003, 5, 643. https://doi.org/10.1016/S1293-2558(03)00034-7
  46. Marchewka, M. K.; Drozd, M., in preparation.
  47. Marchewka, M. K. Acta Chim. Slov. 2003, 50, 239.
  48. Marchewka, M. K.; Drozd, M.
  49. Acta Chim. Slov. v.50 Marchewka, M. K.

Cited by

  1. adsorption in a dually functionalized microporous metal–organic framework vol.3, pp.9, 2015, https://doi.org/10.1039/C4TA05524A
  2. The structure, vibrational spectra and nonlinear optical properties of neutral melamine and singly, doubly and triply protonated melaminium cations—theoretical studies vol.716, pp.1, 2004, https://doi.org/10.1016/j.theochem.2004.11.020
  3. FT-IR, FT-Raman, and DFT computational studies of melaminium nitrate molecular-ionic crystal vol.1034, pp.None, 2004, https://doi.org/10.1016/j.molstruc.2012.10.046
  4. Growth, crystalline perfection, optical, thermal, laser damage threshold and electrical characterization of melaminium levulinate monohydrate single crystal vol.426, pp.None, 2015, https://doi.org/10.1016/j.jcrysgro.2015.05.025
  5. Molecular structure, vibrational spectra and DFT computational studies of melaminium N-acetylglycinate dihydrate vol.1121, pp.None, 2004, https://doi.org/10.1016/j.molstruc.2016.05.059
  6. The Role of Free Radicals in Hemolytic Toxicity Induced by Atmospheric-Pressure Plasma Jet vol.2017, pp.None, 2004, https://doi.org/10.1155/2017/1289041
  7. Solid-state supramolecular architectures formed by co-crystallization of melamine and 2-, 3- and 4-fluorophenylacetic acids vol.1152, pp.None, 2004, https://doi.org/10.1016/j.molstruc.2017.09.099