습식 분해법을 이용한 해산물 중 총 비소 분석을 위한 전처리 방법 연구

Study on the Pretreatment of Seafood for the Determination of Total Arsenic using Wet Ashing Method

  • 김선태 (한국과학기술연구원 특성분석센터) ;
  • 박경수 (한국과학기술연구원 특성분석센터)
  • Kim, Sun Tae (Advanced Analysis Center, Korea Institute of Science and Technology) ;
  • Park, Kyung Su (Advanced Analysis Center, Korea Institute of Science and Technology)
  • 투고 : 2003.09.09
  • 심사 : 2003.10.16
  • 발행 : 2003.12.25

초록

Pretreatment method for the determination of total arsenic in seafood sample was studied. NIST SRM 1566a oyster tissue ($14.0{\pm}1.2mg\;As/kg$) as a standard arsenic compound in order to establish the decomposition method. We confirmed that the best way for pretreatment of seafoods to analyze total arsenic content precisely was $HNO_3-H_2SO_4-HCIO_4$ method by comparison of two methods which are dry ashing and wet ashing methods.

키워드

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