Analytical Science and Technology (분석과학)

The Korean Society of Analytical Sciences (한국분석과학회)
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Determination of fungicides in wines by solid-phase extraction and gas chromatography with mass selective detection

고체상 추출법과 GC/MS를 이용한 포도주 중의 fungicides 정량

  • Park, Gyo-Beom (Chemical Analysis Laboratory, Korea Research Institute of Chemical Technology) ;
  • Lee, Sueg-Geun (Chemical Analysis Laboratory, Korea Research Institute of Chemical Technology)
  • Received : 2003.09.15
  • Accepted : 2003.09.26
  • Published : 2003.12.25
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Abstract

The fungicides, used for grape growth and remained in the wine products from domestic and foreign countries such as vinclozolin, dichlofluanid, penconazole, procymidone were quantitatively analyzed after solid-phase extraction using a GC/MS-SIM method. The results obtained were as follows: for all the samples, the content of procymidone was in the range from 2.2 to $76.1{\mu}g/L$, recoveries 81.3-93.1 %, and standard deviation 1.4-3.4 %.

본 연구에서는 우리나라에서 시판되고 있는 국내 및 외제 와인에 대하여 vinclozolin, dichlofluanid, penconazole, procymidone 등의 살균제 잔류함량을 고체상 추출법을 이용한 GC/MS-SIM 방법으로 정량 하였다. 분석결과 모든 시료에서 procymidone의 함량이 $2.2-76.1{\mu}g/L$가 검출되었고, 회수율은 81.3-93.1 %, 표준편차는 1.4-3.4 %로 나타났다.

Keywords

References

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