Textile Science and Engineering (한국섬유공학회지)

The Korean Fiber Society (한국섬유공학회)
권호 표지

Effects of Crystallization Temperature on the Thermal and Mechanical Properties of PEEK Films

결정화 온도가 PEEK 필름의 열적 및 기계적 성질에 미치는 영향

  • 나성기 (서울대학교 생물자원공학부) ;
  • 박종신 (서울대학교 생물자원공학부)
  • Published : 2003.06.01
⟨ Previous Next ⟩

Abstract

The morphology and related properties have been studied for the thermoplastic semicrystalline poly(phenyletheretherketone), PEEK, film crystallized at different temperatures. Semicrystalline PEEK films were obtained by cooling the melt to different temperatures using the amorphous films. The semicrystalliile films were characterized using differential scanning calorimetry, X-ray diffraction, tensile testing and dynamic mechanical analysis. A polarizing microscope was used to examine crystalline morphology. Crystallization temperature and degree of crystallinity affected the tensile and dynamic mechanical properties. The analysis of thermal, X-ray diffraction, and tensile properties of the semicrystalline films indicates that the film crystallized at 25$0^{\circ}C$ exhibited the highest crystallinity and very tough behavior compared with other semicrystalline films.

Keywords

References

  1. J. Mat. Sci. v.27 Evaluation of Interfacial Properties between Carbon Fibres and Semicrystalline Thermoplastic Matrices in Single-Fibre Composites N.Ogata;H.Yasumoto https://doi.org/10.1007/BF01105281
  2. Polym. Eng. Sci. v.26 Crystallization Kinetics of Poly-Ether-Ether-Ketone(PEEK) Matrices C.N.Veliasaries;J.C.Seferis https://doi.org/10.1002/pen.760260111
  3. Comp.Sci.Technol. v.35 Failure Mechanism in Continuous Carbon-Fiber Reinforced PEEK Composites P.J.Hine;B.Brew;R.A.Duckett;I.M.War https://doi.org/10.1016/0266-3538(89)90069-9
  4. Polym. Comm. v.25 The Structure of Crystalline PEEK J.N.Hay;D.J.Kimmish;J.I.Langford;A.I.M.Rae
  5. Eur. Polym. J. v.30 Trandcrystalline Structure of PEEK Z.Hanmin;Z.Zhiyi;P.Weizou;P.Taiyou https://doi.org/10.1016/0014-3057(94)90165-1
  6. Polymer v.40 Crystallization Kinetics of Poly(ether ether ketone)(PEEK)from Its Metastable Melt S.Tan;A.Su;J.Luo;E.Zhou https://doi.org/10.1016/S0032-3861(98)00275-4
  7. Polymer v.24 The Morphology of Poly(arylether-ether-ketone) D.J.Blundell;B.N.Osborn https://doi.org/10.1016/0032-3861(83)90144-1
  8. J. Appl. Polym. Sci. v.64 Tensile Mechanical properties of PEEK Films Over a Wide Range of Strain Rates(Ⅱ) N.D.Alberola;P.Mele;C.Bas https://doi.org/10.1002/(SICI)1097-4628(19970509)64:6<1053::AID-APP3>3.0.CO;2-K
  9. J. Appl. Polym. Sci. v.63 Frictional Surface Temperature Determination of High-Temperature-Resisitant Semicrystalline Polymers by Using Their Double Melting Features M.Q.Zhang;L.Song;H.M.Zeng;K.Friedrich;J.Karger-Kocsis https://doi.org/10.1002/(SICI)1097-4628(19970131)63:5<589::AID-APP6>3.0.CO;2-Q
  10. J. Appl. Polym. Sci. v.33 Effect of Thermal History on Mechanical Properties of Polyetheretherketone below the Glass Transition Temperature P.Cebe;S.Y.Chung;S.Hong https://doi.org/10.1002/app.1987.070330217
  11. J. Appl. Polym. Sci. v.33 Annealing Effects on the Crystallinity of Polyetheretherketone(PEEK) and Its Carbon Fiber Composite G.M.K.Ostberg;J.C.Seferis https://doi.org/10.1002/app.1987.070330103