DOI QR코드

DOI QR Code

A STUDY ON THE DEGREE OF CONVERSION OF LIGHT CURING COMPOSITE RESIN ACCORDING TO THE THICKNESS OF TOOTH STRUCTURE PENETRATED BY LIGHT AND APPLIED LIGHT CURING TIME

조사광이 통과하는 치질의 두께와 광조사시간에 따른 광중합형 복합레진의 중합률에 관한 연구

  • Hwang, Kee-Hwan (Department of Conservative Dentistry & Institute for Oral Bioscience, College of Dentistry, Chonbuk National University) ;
  • Jang, In-Ho (Department of Conservative Dentistry & Institute for Oral Bioscience, College of Dentistry, Chonbuk National University) ;
  • Lee, Se-Joon (Department of Conservative Dentistry & Institute for Oral Bioscience, College of Dentistry, Chonbuk National University) ;
  • Lee, Kwang-Won (Department of Conservative Dentistry & Institute for Oral Bioscience, College of Dentistry, Chonbuk National University)
  • 황기환 (전북대학교 치과대학 치과보존학교실 및 구강생체과학연구소) ;
  • 장인호 (전북대학교 치과대학 치과보존학교실 및 구강생체과학연구소) ;
  • 이세준 (전북대학교 치과대학 치과보존학교실 및 구강생체과학연구소) ;
  • 이광원 (전북대학교 치과대학 치과보존학교실 및 구강생체과학연구소)
  • Published : 2002.01.01

Abstract

Physical properties of composite resins such as strength, resistance to wear, discoloration, etc depend on the degree of conversion of the resin components. The purpose of this study was to evaluate the degree of conversion of the composite resins according to the thickness of tooth structure penetrated by light and applied light curing time. The coronal portions of extracted human teeth (one anterior tooth, three posterior tooth) was embedded by pink denture material. the mounted teeth were cut into three illumination sections (1mm thickness enamel section, 1mm thickness dentin section, 2mm thicknes dentin section) and one backing section with cutting wheel. Thin resin films were made by using 6kg pressure between slide glass during 5 minutes Thin resin film was light cured on coupled illumination section during 40sec, 80sec and 120sec. each illumination section was coupled as follows; no tooth structure(X), ename section(E), enamel section + 1mm dentin section(ED1), enamel section + 2mm dentin section(ED2), enamel section + 1mm dentin section + 2mm dentin section(EDD). To simulate the clinical situation more closely, thin resin films was cured against a backing section of tooth structure. The degree of conversion of carbon double bonds to single bonds in the resin films were examined by means of Fourier Transform Infrared Spectrometer. The results were obtained as follows ; 1 As curing time was increased, conversion rate was increased and as tooth thickness which was penetrated by curing light was increased, conversion rate was decreased. 2. At all tooth thickness groups, conversion rate between 80sec and 120sec was not significantly increased(P>0.05). 3. At 40sec group and 80sec, conversion rate between no tooth structure(X) group and 1mm enamel section(E) group was not significantly decreased(P>0.05). 4. At 80sec group and 120sec, conversion rate between 1mm enamel section(E) group and 1mm enamel section + 1mm dentin section(ED1) group was not significantly decreased(P>0.05).

Keywords

References

  1. Cook. W.D.: Factor affecting the depth of cure of UV-polymerized composites. J. Dent. Res. 59:800-808. 1980 https://doi.org/10.1177/00220345800590050901
  2. Reinhardt. K.J., VAhl, J.: Zur Frage der Aushartung und photo polymeriaierbarer kpmposiste in Unterschnitten. Dtsch. Zan-naorztl. 36:8-10, 1981
  3. Inai Y. et al.: The importance of polymerization initiator system and interfacial initiation of polymerization in adhesive bonding of resin to dentin. J. Dent. Res. 70:1088, 1991
  4. Ruyter, I.E., Svendsen, S.A.: Remaining methacrylate group in composite restorative materials. Acta Odontol Scand. 36:75-82, 1978 https://doi.org/10.3109/00016357809027569
  5. Grassie, N.: Chemistry of high polymer degradation process. Bulter worth pub. 255: 1956
  6. Ruyter, I.E., Oyased. H.: Compressive creep of light cure resin based restorative materials. Acta Odontol. Scand.: 40: 359-364, 1982 https://doi.org/10.3109/00016358209024081
  7. Inoue. K, Hayashi, I.: Residual monomer(Bis-GMA) of composite resin. J. Oral. Rehab. 9:493-497, 1982 https://doi.org/10.1111/j.1365-2842.1982.tb01039.x
  8. Cook, W.D.: Spectral distributions of dental photopolymerization source. J. Dent. Res. 61:1436-1438, 1982 https://doi.org/10.1177/00220345820610121201
  9. Jordan. R.: Esthetic composite bonding. technique and materials. 20: 2nd edit.: Mosby Year Book
  10. Heigl, J.. Bell, M. and White. J.: Application of infrared spectroscopy to the analysis of liquid hydrocarbon. Analytical chemistry, 19. 293 https://doi.org/10.1021/ac60005a003
  11. Bowen, R.L.: Dental filling material comprising vinylsilane treated fused silica and a binder consisting of the reaction product of bisphenol and glycidyl methacrylate. US Patent 1962, 3, 066, 112
  12. Full, C.A., Hollander. W.R.L: The composite resin restoration. A literature review part III. what the future holds. J. Dent. Child 60: 57~60, 1993
  13. Rerracnace, J.L.: Using posterior composites appropriately. J. Am. Dent. Assoc 123: 53-58. 1992
  14. Ruyter. I.E.: Monomer systems and polymerization. In: posterior composite resin. dental restorative materials Vanherle, G. and Smith, D.C., Eds., Amsterdam: Peter Szule Publishing Co., pp 109-126, 1985
  15. Mannual of Z-100 composites
  16. Ruyter. I. E.. Oysaed. H.: Conversion in different depth of ultraviolet and visible light actived composite materials. Acta Odontol. Scand. 40:179-192,1982 https://doi.org/10.3109/00016358209012726
  17. Peter, K.. Ralf K: Effect of sequential versus continuous irradiation of a light-cured resin composite on shrinkage. viscosity, adhesion and degree of polymerization. American J. of Dent. vol 11. No 1: 17-23
  18. 양홍서, 박영준 복합레진의 조성변화가 물리적 성질에 미치는 영향에 관한 연구, 대한치과의사협회지, 27:185-199, 1989
  19. Swarz. M.L.. Phillips, R.W.. Rhodes, B.: Visible light activate resins-depth of cure. J. Dent. Res. 61 :270. 1982
  20. Ferrancance, J.L .. Greener, E.H.: Fourier transform infrared analysis of polymerization in unfilled resins. methods comparision J. Dent. Res. 63: 1093, 1984 https://doi.org/10.1177/00220345840630081901
  21. 김덕, 민병순, 최호영, 박상진, 최기운: 아르곤 레이저에 의한 복합레진의 중합 시 물성변화에 관한 연구 대한치과보존학회지 23(1):1-20 , 1998
  22. Chung, K.. Greener, E.H.: Degree of conversion of seven visible light-cured posterior composites. J. Oral Rehab. 15:555-560, 1988 https://doi.org/10.1111/j.1365-2842.1988.tb00192.x
  23. Koenig, J. L.: Fourier transform infrared spectroscopy of polymers 89-147, Advances in polymer science
  24. Guerra, R. M. et al: FTIR monomer conversion analysis of UDMA-based dental resins. J. Oral Rehab. 23:632-637, 1996
  25. 김경현, 권오승, 김현기, 백규철, 엄정문, 권혁춘: 수종의 광중합 복합레진의 중합깊이와 광조사시간에 따른 중합률에 관한 연구. 대한치과보존학회지 22:1:35-53. 1997
  26. 문은재, 김병현, 조병훈, 권혁춘: 실험적 접착레진의 단량체 조성비에 따른 중합률 및 전단결합강도에 관한 연구. 대한치과보존학회지 24:1: 1999
  27. Anne Peutzfeldt: Resin composite in dentistry: the monomer systems E. J. oral Sci. 105: 97-116 1997 https://doi.org/10.1111/j.1600-0722.1997.tb00188.x
  28. Asmussen, E.: Factors affecting the quantity of remaining double bond in restorative resin polymers. J. Dent. Res. 90:490-496. 1982
  29. A. Peutzfeldt: Quantity of remaining double bonds of propanal-containing resins J. Dent. Res. 73(10): 1657-1662. 1994 https://doi.org/10.1177/00220345940730101101
  30. Eliades. G.G., Vougiouklais. G.J., Caputo. A.A.: Degree of double bond conversion in light cured composites. Dent. Mat. 3: 19-25. 1987 https://doi.org/10.1016/S0109-5641(87)80055-6
  31. Z. Tarle. A. Meniga. M. Ristic. J. Sutalo. G.Pichler. C.L. Davidson: The effect of the photopolymerization method on the quality of composite resin samples. J. Oral. Rehab. 25:436-442. 1998 https://doi.org/10.1046/j.1365-2842.1998.00258.x
  32. Fan. P.L .. Stanford. C.M.: Effect of backing reflectance and mold size on polymerization of photoactivated composite resin. J. Dent. Res. 63:1245-1247, 1984 https://doi.org/10.1177/00220345840630101601
  33. Standlee. J.P .. Caputo. A.A.. Hokama. S.N.: Light cured composites. Calif. Dent. J. 16:25-28, 1988
  34. Weaver, W.S.. Blank. L.W.. Pelleu. G.B.: A visible light activated resin cured through tooth structure. Gen. Dent. 36:136-137, 1988

Cited by

  1. Surface hardness of the dental composite cured by light that penetrate tooth structure according to thickness of tooth structure, light intensity and curing time vol.30, pp.2, 2005, https://doi.org/10.5395/JKACD.2005.30.2.128