감귤류와 한국산 청피에 함유된 Methoxylated Flavonoids의 분석과 정량적 분포

Quantitative Distribution and Analysis of Methoxylated Flavonoids in Citruses and Korean Chung-pi

  • Baik, S.O. (Korea Ginseng and Tobacco Research Institute) ;
  • Bock, J.Y. (Korea Ginseng and Tobacco Research Institute) ;
  • Chun, H.J. (Professional graduate School of Oriental Medicine, Wonkwang Univ.) ;
  • Jeong, S.I. (Professional graduate School of Oriental Medicine, Wonkwang Univ.) ;
  • Han, W.S. (Chemistry Dept., Mokwon Univ.) ;
  • Kim, I.K. (Korea Ginseng and Tobacco Research Institute)
  • 투고 : 2001.06.26
  • 발행 : 2001.08.25

초록

감귤류와 한국산 청피에 함유된 methoxylated flavonoids (sinenstin, nobiletin, tangeretin)를 HPLC, mass 그리고 NMR로 분리하고 분석하였다. Methoxylated flavonoids는 Chung-pi(I)과 Chung-pi(II)에 가장 풍부하게 함유되었다. 한국산 밀감에서 얻어진 Chung-pi(I), (II)의 methoxylated flavonoids 함유량은 밀감성숙도에 따라 증가하였으며, 10월 중순이후에는 서서히 감소하였다.

Methoxylated flavonoids (sinenstin, nobiletin, tangeretin) were isolated and identified by preparative HPLC, mass and NMR. Chung-pi(I) and Chung-pi(II) contained methoxylated flavonoids most richly. Methoxylated flavonoids in Chung-pi obtained from Korean Milgam increased with fruit maturity, while contents of the methoxylated flavonoids gradually decreased after mid of October.

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