A Study On Crystalline Structure Change by Isothermally Annealed after Elevated heating of drawn PP filaments

연신한 PP filament의 승온열처리에 의한 결정구조 변화에 관한 연구

The change of crystalline structure of drawn PP filaments were investigated. Samples were treated by isothermally annealed after elevated heating from $20^{\circ}C$. Measurements were carried out with XRD for crystallite size and density gradient tube for crystallinity. Isothermally heat treatment were carried out at the temperature of $100^{\circ}C$, $120^{\circ}C$ and $140^{\circ}C$ for 10min., 30min. and 60min. in dry oven. The isothermal heat treatment after elevated heating from $20^{\circ}C$ were carried out at the temperature of $100^{\circ}C$, $120^{\circ}C$ and $140^{\circ}C$ for 10min., 30min. and 60min. with heating rate of $1^{\circ}C$/min., $5^{\circ}C$/min. and $10^{\circ}C$/min. From the results of this study, it found the following facts. It was found that the crystallinity and crystallite size of (110) plane of sample were increased with increasing of annealed temperature and time. Also crystallinity and crystallite size of samples which were isothermally annealed after elevated heating from $20^{\circ}C$ were higher than those of isohtermally annealed samples.