The growth YMnO$_3$ single crystals using a floating zone method

부유대용융법에 의한 YMnO$_3$단결정 성장

  • 권달회 (한양대학교 세라믹 공학과) ;
  • 강승구 (경기대학교 신소재공학과) ;
  • 김응수 (경기대학교 신소재공학과) ;
  • 김유택 (경기대학교 신소재공학과) ;
  • 심광보 (한양대학교 세라믹 공학과)
  • Published : 2000.08.01

Abstract

High quality crystals of $YMnO_3$, which is interested in non-volatile memory device application, were grown by the floating zone method. Optimum condition for powder synthesis was established to be $1200^{\circ}C$ for 10 hrs and optimum condition for sintering of $YMnO_3$feed-rod was established to be $1500^{\circ}C$ for 10hrs respectively. It was found from non-seeded growth experiment that $YMnO_3$crystal was grown preferentially to the [1010] orientation. The $YMnO_3$single crystal, which was grown to the direction of perpendicular to C-axis, was typically 5mm in diameter, 50 mm in length and showed dark-blue color.

부유대용융법에 의해 비휘발성 기억소자용 강유전성물질인 $YMnO_3$단결정을 육성하였다. 결정성장전 YMnO$_3$분말의 최적합성조건은 $1200^{\circ}C$에서 10시간, 최적원료봉 소결조건으로 $1500^{\circ}C$에서 10시간이었다. 초기 Seed가 없는 상태에서의 실험에서 성장된 단결정의 우선성장방위는 X-ray Laue분석을 통하여 [1010] 임을 알수 있었고 이 결정을 seed로 사용하여 c-축에 수직한 방향으로 $YMnO_3$단결정을 성장하였다 성장된 단결정은 직경 5mm, 길이 50 mm로 양질의 흑청색 결정이었다.

Keywords

References

  1. Ferroelectrics and Related Substances, Oxides v.16 no.a Ladolt-Bornstein Numerical Data and Functional Relationships in Science and Technology, New Series, Group 3 T. Mitsui;S. Nomura;K.-H Hellwege (ed.)
  2. C. R. Acad. Sci v.256 E.F. Bertaut;F. Forrat;P.H. Fang
  3. Phys. Rev B v.56 Z.J. Huang;Y. Cao;Y.Y. Sun;Y.Y Xue;C.W. Chu
  4. J. Phys. Soc of Japan v.67 no.9 Nobuyuki Iwata;Kay Kohn
  5. Appl. Phys. Lett v.69 N. Fujimura;T. Ishida;T. Yoshimura;T. Ito
  6. J. Appl. Phys v.80 N. Fuhimura;S. Azuma;N. Aoki;T. Yoshimura;T. Ito
  7. Appl. Phys. Lett v.74 H.N. Lee;Y.T. Kim;Y.K. Park
  8. Mat. Res. Soc. Symp. Proc v.495 G. Teowee;K.C. McCarthy;F.S. McCarthy;B.H. Dietz;D.G. Davis Jr;D.R. Uhlmann
  9. Abstract of 1999 Material Research Society Spring Meeting W.C. Yi;C.S. Seo;S.I. Kwon;J.G. Yoon
  10. J. Am. Ceram. Soc v.81 no.5 H. Kitahata;K. Tadanaga;T. Minami;N. Fujimura;T. Ito
  11. Crystal Growth Principles and Progress A.W.Vere
  12. Floating Zone Silicon W. Keller;A. Muhlbauer
  13. Advanced Crystal Growth (ISCG6) 6-11 R.A.Brown
  14. J. Crystal Growth v.44 S. Kimura;I. Shindo;K. Kitamura;Y. Mori