The Korean Journal of Ceramics

The Korean Ceramic Society (한국세라믹학회)
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Synthesis and Characterization of Dense $Ti_{0.5}Zr_{0.5}B_2$ Solid Solutions by Electrically-Stimulated Combustion

  • Lee, H. B. (Department of Inorganic Material Engin., Myong Ji University) ;
  • Kim, S. J. (Department of Materials Science and Metallurgical Engin., Kumoh Natl Univ. of Tech.) ;
  • Y. H. Han (Department of Inorganic Material Engin., Myong Ji University) ;
  • J. E. Garay (Department of Inorganic Material Engin., Myong Ji University) ;
  • Zuhair A. Munir (Department of Chemical Engineering and Materials Science University of California Davis)
  • Published : 2000.06.01
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Abstract

Solid solutions of Ti$_{0.5}$Zr$_{0.5}$B$_2$were successfully synthesized and densified simultaneously from elemental reactants by the use of a field-activated, pressure-assisted synthesis method. The method involves the application of an electric current and mechanical pressure across reactant compacts to achieve combustion synthesis. Dense solid solutions with relative densities of up to 99% were produced and characterized by XRD, SEM, and EPMA methods. With a maximum measured temperature of 145$0^{\circ}C$ under a load of 86 MPa for 30 min, the desired dense solid solution wad synthesized.

Keywords

References

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