DOI QR코드

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다이머산 합성 및 공업적 응용성(제1보);점토촉매하에서 다이머산의 합성

Synthesis and Industrial Application of Dimer Acid(1);Synthesis of Dimer Acid with Clay Catalyst

  • 윤영균 (충북대학교 공과대학 공업화학과) ;
  • 정노희 (충북대학교 공과대학 공업화학과) ;
  • 남기대 (충북대학교 공과대학 공업화학과)
  • Yoon, Young-Kyoon (Dept. of Ind. and Eng. Chem., College of Chem., Chungbuk Nat. Univ) ;
  • Jeong, Noh-Hee (Dept. of Ind. and Eng. Chem., College of Chem., Chungbuk Nat. Univ) ;
  • Nam, Ki-Dae (Dept. of Ind. and Eng. Chem., College of Chem., Chungbuk Nat. Univ)
  • 발행 : 1999.06.30

초록

A synthesis of Dimer acid was studied from a tall oil fatty acid. Catalytic activity measured as reactant conversion in a autoclave reactor increase in accordance with the acidity. The optimization of process conditions were tested by an experimental design method. Optimization synthetic conditions of dimer acid and were reaction of tall oil fatty acid during 2 hour at $250^{\circ}C$, used of 7.3 wt% active clay and $1.2{\sim}1.4wt%$ water, and found reation pressure $8{\sim}9Kg/cm^2$. The maximum conversion rate was researched $74{\sim}76%$.

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