Effect of Coagulants on Morphology and Mechanical Properties of Wet-Spun PVC Fiber

습식방사법으로 제조된 PVC 섬유의 형태와 기계적 물성에 미치는 응고제의 영향

  • 이수임 (창원대학교 공업화학과) ;
  • 박성실 (창원대학교 공업화학과) ;
  • 오영세 ((주) 한일합섬 기술연구소)
  • Published : 1999.09.01

Abstract

The effect of coagulation conditions on the morphology of as-spun PVC fibers from wet-spinning was studied with two different coagulant system ($H_2O$/DMF and $H_2O$/MeOH). The morphology of as-spun fibers spun into $H_2O$/DMF became denser but more unsymmetrical in shape with increasing DMF concentration up to 40%. However, the maximum draw ratio, $DR_{max}$, of such as-spun fibers was too low to produce a PVC fiber successfully. On the other hand, the morphology of as-spun fibers spun into $H_2O$/MeOH changed from circular to kidney bean shape with less voids and their $DR_{max}$ also increased with increasing MeOH concentration. $H_2O$/MeOH=20/80 coagulant bath system was suitable for the production of better quality PVC fiber having a denser circular morphology and a high $DR_{max}$ resulted in stronger tensile strength.

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