초록
13Cr-1.5Nb-Fe합금분말이 수분사법으로 제조되엇다. 제조된 합금뷴말을 압축기를 이용하여 ring현상으로 성형한후, 진공중에서 소결하였다. as-prepared 분말의 현상, 입도분포, 성분분석 및 포화자화물 조사하였으며, 소결된 시편의 투자율, 교류자기이력손실이 조사되었다. as-prepared 13Cr-1.5Nb-Fe합금분말의 포화자화는 160emu/g이었으며, 산소함유량은 약 600ppm이었다. 입도분포는 약 70$\mu$m에서 50%vol.을 나타낸다. 교류투자율은 소결온도 및 성형온도가 증가할수록 증가한다. 주파수 20KHz에서 교류자기이력손실은 12ton/cm2성령압력 및 120$0^{\circ}C$ 소결온도 조건에서 107W/cc로 가장우수하다.
13Cr-1.5Nb-Fe alloy powder was fabricated by water atomization method, and ring-shape specimen of this composition was fabricated by oil press, and then sintered in the vacuum furnace. Powder shape, size distribution, composition (C, N, O, S) analysis and saturation magnetization of as-prepared 13Cr-1.5Nb-Fe alloy powder were investigated. Ac permeability and power loss was measured after forming and sintering process. Saturation magnetization and contents of oxygen of the alloy powder is160 emu/g and about 6000 ppm, respectively. 50 % volume fraction indicate particle size of 70$\mu$m. The ac permeability of sintered specimen increases with increasing sintering temperature and forming pressure. The power loss is 107 W/cc at sintering temperature of 1200 $^{\circ}C$, 12 ton/$\textrm{cm}^2$ forming pressure, and 20 KHz. It is the lowest among the prepared specimen.