한국세라믹학회지 (Journal of the Korean Ceramic Society)

  • 제35권8호
  • /
  • Pages.843-849
  • /
  • 1998
  • /
  • 1229-7801(pISSN)
  • /
  • 2234-0491(eISSN)
한국세라믹학회 (The Korean Ceramic Society)
권호 표지

알콜탈수법에 의한 Mn-Zn Ferrite 분체제조 및 소결특성

Synthesis of Mn-Zn Ferrite Powder by Alcoholic Dehydration and Properties of Sintered Body

  • 이대희 (경북대학교 무기재료공학과) ;
  • 김창현 (가야대학교 공학부 세라믹공학과) ;
  • 이병교 (경북대학교 무기재료공학과)
  • 발행 : 1998.08.01
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초록

Fine powders of Mn-Zn ferrite were prepared by the alcoholic dehydration method and densification beha-vior of synthesized powder was investigated. The concentration and pH of solution for optimal precipitation was 0.4M and 2.5 respectively. The spinel single phase metastable state was formed by thermal decom-position of precipitate and then spinel phase was disintegrated into hematite and spinel {{{{ { { ZnFe}_{2 }O }_{4 } }} at 600$^{\circ}C$ With increase of temperature reaction of solid solution between hematite and spinel was proceeded and resulted in the spinel single phase (Mn, Zn Fe){{{{ { {Fe }_{2 }O }_{4 } }} On account of high reactivity of uncalcined powders densification started at 200$^{\circ}C$ lower and completed at 50$^{\circ}C$ lower in comparison with calcined powders.

키워드

참고문헌

  1. Soft Ferrites Properties and Applications(2nd ed.) E. C. Snelling
  2. 자성재료 심포지움 논문집 고투자율 Soft Ferrite의 최신기술 동향 허원도
  3. Am. Ceram. Soc. Bull. v.74 no.4 Soft Ferrite Processing J. A. T. Taylo; S. T. Reczek;A. Rosen
  4. J. Kor. Ceram. Soc v.30 no.6 공침법에 의한 Mn-Zn Ferrite 분말제조 연구 엄태형;고성만;서동수;양준환;박균하
  5. J. Kor. Ceram. Soc. v.30 no.1 습식합성에 의한 Mn-Zn Ferrite의 생성반응에 관한 연구 이경희;이병하;허원도;황우연
  6. Am. Ceram. Bull. v.60 no.2 Nonconventional Powder Preparation Technique D. W. Johnson Jr
  7. J. Am. Ceram. Soc. v.78 no.9 Hydrothernal Synthesis of Manganese Zinc Ferrites M Rozman;M. Drofenik
  8. Ceramic Powders Preparation of Active Powder for Electronic Ceramics by Alcoholic Dehydration of Citrate Solution C. E. Li;H. Y. Ni;B. W. Yin
  9. J. Am. Ceram. Soc. v.71 no.2 Preparation of Manganess Zinc Ferrite Powders by Alcoholic Dehydration of Citrate/Formate Solution P. Sainamthip;V.R.W. Amarakoon
  10. Ceramics Fabrication Process Jap. Ceram. Soc.
  11. Ceramic Fine Powder Technology New Glass Series Editorial Committee
  12. J. Kor. Ceram. Soc. v.32 no.10 알콜탈수법에 의한 Mn-Zn Ferrite 분체제조시 pH의 영향 김창범;신효순;이대희;김창현;이병교
  13. Proceedings of the Fifth International Conference on Ferrites Structural and Oxidation State Transformations during Sintering of Mn-Zn Ferrite D. Le. Roux;F. Onno;P. Perriat
  14. X線回折의 基礎 한봉희
  15. J. Mater. Sci v.24 Reactive Sintering of Manganese Ferrite F. J. C. M. Toolcnaar;M T Van Lierop-Verhees
  16. Ceram. Int. Interaction of (MnZn)O Solid Solutions with Fe₂O ₃as Intermediate Stage of Fornation of Mn-Zn Ferrites V. V. Pan'kov
  17. J. Kor. Ceram. Soc. v.27 no.5 망간징크 페라이트 단결정의 산화;환원반응에 따른 미세구조의 변화 윤상영;김문규