Solid State Polymerization of Poly(ethylene terephthalate)

폴리에틸렌테레프탈레이트의 고상중합에 관한 연구

  • Published : 1997.10.01

Abstract

Solid state polymerization of poly(ethylene terephthalate) (PET) has been carried out under reduced pressure of 0.2 torr at the various temperatures ranging from 200 to 23$0^{\circ}C$. The increase in the molecular weight of resulting polymer has been observed, i.e., the higher molecular weight of the resulting polymer with higher temperature and longer reaction time. It has been found that the linear dependence of the rate of molecular weight increase on reaction time in the early stage of the reaction is no longer valid when the number average molecular weight of the polymer reaches value of 30, 000. The change in the crystal structure and crystallization process has been interpreted by means of density measurement, X-ray diffraction and DSC.

Keywords

References

  1. U. S. Patent 3, 075, 952 Coover
  2. U. S. Patent 3, 051, 212 Daniels
  3. Polym. Eng. Sci. v.10 T. M. Chang
  4. J. Polym. Sci. v.25 S. Chen;F. Chen
  5. Ind. Eng. Chem. v.16 B. D. Whitehead
  6. J. Appl. Polym. Sci. v.32 S. A. Jabarin;E. A. Lofgren
  7. Solid State Behavior of Linear Polyesters and Polyamides J. M. Schultz;S. Fakiroc(Ed.)
  8. J. Appl. Polym. Sci. v.28 C. Chang;M. Sheu;S. Chen
  9. Proc. R. Soc. (London) v.A226 R. de P. Daubeny;C. W. Bunn;C. J. Brown
  10. J. Appl. Polym. Sci. v.22 R. Huisman;H. M. Heuvel
  11. J. Appl. Polym. Sci. v.22 R. Huisman;H. M. Heuvel