Studies on the Optimum Surface Treatment Conditions and the Interfacial Bond Strength of Nylon 6/Glass Fiber Composites

Nylon 6/유리섬유 복합재료의 표면처리 최적조건과 계면결합력에 관한 연구

  • 나성기 (서울대학교 천연섬유학과) ;
  • 박홍신 (제일모직 화성연구소, 효성T&C 중앙연구소)
  • Published : 1997.05.01

Abstract

${\gamma}$-APS (${\gamma}$-aminopropyltriethoxysilane), one of the silane coupling agents, was used to treat glass fiber surfaces to modify the interphase between fiber and matrix. FT-lR (Fourier Transform Infrared) and XPS (X-ray Photoelectron Spectroscopy) were used to characterize functional groups and atoms, respectively, adsorbed on the fiber surface treated by ${\gamma}$-APS. The adsorbed amount of ${\gamma}$-APS on the fiber surface was measured as a function of concentration, pH, treatment time and treatment temperature. The single glass fiber treated at various treatment conditions was embedded between nylon 6 films to make a single fiber embedded specimen which was used to assess the interfacial shear strength by fragmentation test.

Keywords

References

  1. Polymer Science and Technology J. R. Fried
  2. J. Comp. Mater. v.1 O. K. Johannson;F. O. Stark;G. E. Vogel;R. M. Fleischmann
  3. J. Colloid Interface Sci. v.36 J. L. Koenig;P. T. K. Shih
  4. Adhesion and Bonding in Composite Materials R. Yosomiya;K. Morimoto
  5. J. Colloid Interface Sci. v.27 L. H. Lee
  6. Annual Book of ASTM Standards, Designation : D 1708 v.08.02
  7. Fiber-Reinforced Composites; Materials, Manufacturing, and Design P. K. Mallick
  8. Adhesion and Bonding in Composites Materials R. Yosomiya;K. Morimoto