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Construction of Low Noise Electrochemical Quartz Crystal Microbalance


Abstract

A new oscillator for electrochemical quartz crystal microbalance (EQCM) was developed by using an operational amplifier without any LC component. The home-made EQCM using this oscillator showed only 0.02 Hz frequency noise at 0.3 s gate time when a 6 MHz AT-cut crystal was used. Pb underpotential deposition on gold substrate in nitric acid media was examined to demonstrate the performance of this EQCM. The derivative of frequency change could be obtained without averaging multiple scans.

Keywords

References

  1. Electroanalytical Chemistry v.17 Buttry, D. A.;Bard, A. J.(ed.)
  2. Anal. Chem. v.61 Deakin, M. R.;Buttry, D. A.
  3. Science v.249 Ward, M. D.;Buttry, D. A.
  4. J. Appl. Phys. v.68 Reed, C. E.;Kanazawa, K. K.;Kaufman, J. H.
  5. Anal. Chem. v.63 Martin, S. J.;Granstaff, V. E.;Frye, G. C.
  6. Anal. Chem. v.65 Lin, Z.;Yip, C. M.;Joseph, I. S.;Ward, M. D.
  7. Langmuir v.9 Yang, M.;Thompson, M.;Duncan-Hewitt, W. C.
  8. Anal. Chem. v.66 Noel, M. A. M.;Topart, P. A.
  9. Electrochim. Acta v.30 Bruckenstein, S.;Shay, M.
  10. J. Electroanal. Chem. v.188 Bruckenstein, S.;Shay, M.
  11. Langmuir v.2 Melroy, O.;Kanazawa, K.;Gordon Ⅱ, J. G.;Buttry, D. A.
  12. J. Electroanal. Chem. v.239 Deakin, M. R.;Melroy, O.
  13. Appl. Optics v.29 Lakkaraju, S.;Bennahmias, M. J.;Borges, G. L.;Gordon Ⅱ, J. G.;Lazaga, M.;Stone, B. M.;Ashley, K.
  14. J. Electrochem. Soc. v.138 Gabrielli, C.;Keddam, M.;Torresi, R.
  15. Anal. Chem. v.65 Nivens, D. E.;Chambers, J. Q.;Anderson, T. R.;White, D. C.
  16. J. Electrochem. Soc. v.140 Rivera, I. M.;Cabrera, C. R.
  17. Anal. Chem. v.65 Lee, W.-W.;White, H. S.;Ward, M. D.
  18. Rev. Sci. Instrum. v.64 Komplin, G. C.;Schleifer, F.;Pietro, W. J.
  19. Anal. Chem. v.66 Bruckenstein, S.;Michalski, M.;Fensore, A.;Li, Z.
  20. Anal. Chem. v.66 Shana, Z. A.;Josse, F.
  21. Anal. Chem. v.67 Mo, Y.;Hwang, E.;Scherson, D. A.
  22. Anal. Chim. Acta. v.142 Nomura, T.;Okuhara, M.
  23. Electrochim. Acta v.34 Bourkane, S.;Gabrielli, C.;Keddam, M.
  24. IEEE Trans. Ultras. Ferroel. Freq. Control v.37 Josse, F.;Shana, Z. A.;Radtke, D. E.;Haworth, D. T.

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  2. Fused‐Silica Capillary Dropping Mercury Electrode for Electrocapillary Measurements vol.25, pp.1, 1996, https://doi.org/10.1002/elan.201200382