Characteristics of PET Microfiber Fabrics Decomposed by Sodium glycerolate/Glycerol Solution

Sodium glycerolate/Glycerol 용액에 의한 PET 신합섬직물의 분해특성

  • Yoon, Jong Ho (Dept. of Industrial Chem., Kyungpook Sanup Univ., Kyungsan, Korea) ;
  • Huh, Man Woo (Dept. of Textile Eng., Kyungpook Sanup Univ., Kyungsan, Korea) ;
  • Bae, Jeong Sook (Dept. of Clothing and Textiles, Taegu Univ., Kyungsan, Korea) ;
  • Cho, Yong Suk (Dept. of Textile Eng., Taegu Hyosung Catholic Univ., Kyungsan, Korea)
  • Published : 1996.04.01

Abstract

Polyester microfiber fabrics were alcoholysed at 120, 140, and 16$0^{\circ}C$ in 0.5, 1.0, and 1.5% of sodiumglycerolate/glycerol solutions(NaGR) up to 80% and the characteristic decomposition features were compared and discussed with the results of the hydrolysis done by 5% sodium hydroxide solution(NaOH) at 80, 90, and 10$0^{\circ}C$. The resulting activation thermodynamic parameters calculated by the combined use of the Arrhenius equation and the Eyring equation were in NaOH case ${\Delta}H^*$=- 13.89 kcal/mol, ${\Delta}S^*$/=-38.12 cal/mol K, and ${\Delta}G^*$=25.25 kcal/mol and in NaGR case ${\Delta}H^*$=29.81 kcal/mol, ${\Delta}S^*$=-2.29 cal/mol K and ${\Delta}G^*$=30.49 kcal/mol. Since in all cases NaGR-PET system has higher activation thermodynamic parameters, it was concluded that NaGR-PET reaction system is more favorable at high temperatures and occurs in a less selective fashion, in comparison to the NaOH-PET reaction system.

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