Effects of Pretreatment Method on the Bonding Strength of 4-META/MMA-TBB Resin to Bovine Dentin

상아질 전처리방법이 4-META/MMA-TBB계 레진의 접착강도가 미치는 영향

  • 김교한 (경북대학교 치과대학 치과재료학교실) ;
  • 김영빈 (경북대학교 치과대학 치과재료학교실, 경북대학교 치과대학 치과보존학교실, 공과대학 고분자공학과)
  • Published : 1995.12.01

Abstract

The present study investigated the effectiveness of pretreatment on dentin bonding. The adhesive resin was 5% 4-methacryloyloxyethyl trimellitate anhydride (4-META) in methyl methacrylate (MMA) combined with poly-MMA powder. Polymerization of this resin was initiated by tri-n-butyl borage (TBB). Ground bovine dentin samples were etched with either an aqueous solution of 10% citric (10-0 solution) (Group I) or aqueous solution of 10% citric acid and 3% ferric chloride(10-3 solution) (Group ll ). After etching, the primer (an aqueous solution of 35% hydroxyethyl methacrylate (HEM- A) and 5% glutaraldehyde was applied on the differently etched surfaces (Group III , Group IV). The 10-0 treatment showed the lowest tensile bond strength, followed by the 10-3 treatment, primer application after the 10-0 treatment and primer application after the 10-3 treatment. The relationship among the surface morphology after pretreatment, fractured surface morphology and tensile bond strength was examined. It revealed that the surface morphology change by different pretreatment influenced the bond strength and the resulting fractured surface morphology. The correlation of tensile bond strength with the fracture morphology was explained.

Keywords

References

  1. J Dent Res v.34 A simple method of increasing the adhesion of acrylic filling materials to enamel surfaces Buonocore,M.G.
  2. J Am Dent Assoc v.107 A method for bonding to dentin and enamel Bowen,R.L.;Cobb,E.N.
  3. Transactions of international congress on dental materials Erickson,R.L.
  4. Dent Mater Dental smear layer: an asset & a liability for bonding White,G.J.;Beech,D.R.;Tyas,M.J.
  5. Prosthet Dent v.61 Interaction between the dentinal smear layer and composite bond strength Ishiok,S.;Caputo,A.A.
  6. J Am Dent Assoc v.64 Tensile strength and modulus of elasticity of tooth structure and several restorative materials Bowen,R.L.;Rodriguez,M.S.
  7. J Dent Res v.61 Adhesion bonding of various materials to hard tissues : Improvement in bond strength to dentin Bowen,R.L.;Cobb,E.N.;Rapson,J.E.
  8. J Dent Res v.68 Substitution for N-phenylglycine in adhesive bonding to dentin Johnston,A.D.;Asumussen,E.;Bowen,R.L.
  9. Rep Inst Dent Mater v.2 Studies on dental self-curing resin Masuhara,E.;Kojima,K.;Hirasawa,J.;Kimura,T.
  10. J Jpn Dent Mater v.5 Study of dental adhesive resin containing phosphoric acid methacrylate monomer Yamauchi,J.
  11. Dent Mater J. v.12 Efficacy of dentin bonding agents combined with self-etching dentin primers containing pheyl-P Tani,C.;Itoh,K.;Hisamitsu,H.;Wakumoto,S.
  12. Kobunshi Ronbunshu v.45 Synthesis of phosphoric compounds and their adhesives to bovine teeth Nakabayashi,N.;Kanda,K.
  13. J Dent Res v.68 Adsorption of 4-META on hydroxyapatite and its role in composite bonding Misra,D.N.
  14. J Jpn Dent Appar Mater v.19 Studies on dental self-curing resin. Adhesion of PMMA with bovine enamel or dental alloys Takeyama,M.;Kashibuchi,N.;Nakabayashi,N.;Masuhara,E.
  15. Am J Dent v.2 Mechanism and clinical implications of bond for mation for two dentin bonding agents Erickson,R.L.
  16. Jpn J Consery Dent v.33 A study on the resin impregnated layer of dentin. Ⅰ. A comparative study on the decalcified and undecalcified sections and the application of argon ion beam etching to disclose the resin imprognated layer of dentin Inokoshi,S.;Hosoda,H.;Harnirattisai,C.;Shimada,Y.;Tatsumi,T.
  17. J Jpn Den Mater v.1 Resin reinforced dentin due to infiltration of monomers into the dentin at the adhesive interface Nakabayashi,N.
  18. J Biomed Mater Res v.16 The promotion of adhesion by the infiltration of monomers into tooth substrate Nakabayashi,N.;Koima,K.;Masuhara,E.
  19. Rep Inst Med Dent Eng v.17 SEM and TEM observation of dentin interface treated for adhesion Nakabayashi,N.;Watanabe,A.
  20. CRC Critic Rev Biocompatibility v.1 Biocompatibility and promotion of adhesion to tooth substrates Nakabayashi,N.
  21. Dent Mater J. v.13 Effect of filler content on bonding efficacy of 4-META/MMA-TBB bonding agent Tani,C.;Itoh,K.;Hisamitsu,H.;Wakumoto,S.
  22. 대한치과보존학회지 v.18 동 및 철이온이 MMA/TBBO 레진의 상아질 접착에 미치는 영향 박진훈
  23. Dent Mater J. v.14 Phosphoric acid tooth conditioner containing copper salt for bonding MMA-TBB resin Park,J.;Imai,Y.
  24. Quintenssence Int v.23 Identification of a resindentin hybrid layer in vital human dentin created in vivo:Durable bonding to vital dentin Nakabayashi,N.;Ashizawa,M.;Nakamura,M.
  25. J Jpn Dent Mater v.8 Formation of photocurable bonding linear and adhesion to dentin. Effect of photoinitiator, monomer and photoirradiation Nikaido,T.
  26. J Dent Res v.70 Vibrational analysis by Raman spectroscopy of the interface between dental adhesive resin and dentin Suzuki,M.;Kato,H.;Wakumoto,S.
  27. J Dent Res v.68 no.733 XPS characterization of dentin and dentin treated with bonding primers Thompson,U.P.;Elder,T.C.;Davis,G.
  28. J Dent Res. v.74 Tensile properties of resin-infiltrated demineralized human dentin Sano,H.;Takatsu,T.;Ciucchi,B.;Russel,C.M.;Pashley,D.H.
  29. J Debt Res. v.72 Comparative SEM and TEM examination of the ultrastructure of the resin-dentin interdiffusion zone Van Meerbeek,B.;Dhem,A.;Goret-Nicaise,M.;Braem,M.;Lambrechts,P.;Vanherle,G.
  30. J Dent Res. v.72 Chemical characterization of the resin-dentin interface by micro-raman spectroscopy Van Meerbeek,B.;Dhem,A.;Goret-Nicaise,M.;Braem,M.;Lambrechts,P.;Vanherle,G.
  31. J Dent Res. v.72 Assessment by nano-indentation of the hardness and elasticity of the resin-dentin bonding area Van Meerbeek,B.;Dhem,A.;Goret-Nicaise,N.;Braem,M.;Lambrechts,P.;Vanherle,G.
  32. J Dent Res v.67 Adhesive 4-META/MMA-TBB opaque resin with poly (methyl methacrylate)-coated titanium dioxide Masuhara,H.;Nakabayashi,N,
  33. J Dent Res v.67 A new ion-coating surface treatment of alloys for dental adhesive resins Tanaka,T.;Hirano,M.;Kawahara,M.;Matsumura,H.;Atsuta,M.
  34. J Jpn Orthod Soc v.46 Study on the direct bonding method for porcelain and ceramic bracker Maeda,M.;Mogi,M.;Miura,F.;Nakabayashi,N.
  35. J Jpn Dent Mater v.10 Bonding of MMA-TBB resins to extracted bovine dentin treated with EDTA 3-2 (NH₄/Fe) Nakabayashi,N.;Takarada,K.;Kojima,M.
  36. J Dent Res v.63 Bond strength between dentin and restorative resins mediated by mixtures of HEMA and Glutaldehyde Munksgaard,E.L.;Asmussen,E.
  37. Scan J Dent Res v.93 Dentin-polymer bond mediated by Glutaraldehyde/HEMA Munksgaard,E.L.;Asmussen,E.
  38. J Jpn Dent Mater v.12 Adhesion of restorative resin to tooth substrate Suzuki,K.;Nakai,H.
  39. Dent Mater v.8 Effect of HEMA on bonding to dentin Nakabayashi,N.;Takarada,K.
  40. Dent Mater v.8 Dentin adhesion of modified 4-META/MMA-TBB resin:function of HEMA Nakabayashi,N.;Watanabe,A.;Gendusa,N.J.
  41. 대한치과보존학회지 v.18 산처리가 상아질 접착에 미치는 영향 김영경;김성교;박진훈
  42. 대한치과보존학회지 v.20 상아질 표면의 건조에 따른 습윤상태가 레진 시멘트의 접착에 미치는 영향 손강하;박진훈;조규증
  43. 대한치과보존학회지 v.20 불소도포가 상아질 접착에 미치는 여향 권형조;박진훈;조규증
  44. 1995 Federation Meeting of Korean Basic Medical Scientists Development of korean dental dentin bonding agent K.H.KIM;J.H.PARK;I.K.KANG
  45. J Jan Dent Mater v.5 The adhesion of resin to dentin and structural change of dentin collagen Mizunuma,T.
  46. Nishihoshi v.28 The 4-META/MMA-TBB resin adhesion of dentin pretreated with EDTA Shimizu,H.;Nakabayashi,N.
  47. J Jpn Dent Mater v.11 Effectiveness of 2-methacryloyloxyethyl methyl sulfoxide (MEMSO) on permeability of demineralized dentin and improvement of bond strength to dentin Ide,K.;Ishihara,K.;Nakabayashi,N.
  48. Adhesive Dentistry v.8 Treatment of dentin by aqueous solution of amino acid deriatives-HEMA Suzuki,K.;Takahashi,M.;Nakai,H.
  49. J Jpn Dent Mater v.12 Adhesiveness of resin to acid-etched dentin Mizuno,Y.;Suzuki,K;Kondo,Y