과제정보
연구 과제 주관 기관 : 한국표준과학연구원
분석과학 (Analytical Science and Technology)
- 제7권4호
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- Pages.555-561
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- 1994
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- 1225-0163(pISSN)
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- 2288-8985(eISSN)
흑연로 원자흡수분광광도법에 의한 뇨시료 중 흔적량 원소의 정량
Determination of Trace Elements in Urine Samples by Graphite Furnace Atomic Absorption Spectrophotometry
- Choi, Chong-Moon (Department of Chemistry, Korea University) ;
-
Choi, Hee-Seon
(Department of Chemistry, University of Suwon)
;
- Park, Chang Joon (Inorganic Analysis Laboratory, Korea Standard & Science Research Institute) ;
- Kim, Young-Sang (Department of Chemistry, Korea University)
- 투고 : 1994.11.02
- 발행 : 1994.12.25
초록
A method was described for the graphite furnace atomic absorption spectrophotometric determination of trace cadmium, copper, chromium and lead in urine samples. The elements were directly determined without any other treatments. The ash temperature was intensively optimized to improve the large background by the removal of organic materials and alkali and alkali earth metals in urine samples. Two kinds of standard solutions were used to plot calibration curves. From the recovery data, it could be confirmed that the analytical results with the synthetic urine matrix similar to real urine were more accurate than with a deionized water matrix.