Regenerated Cellulose Fiber from Cellulose/Trifluoroacetic Acid/Methylene Chloride Solution

셀롤로오스/삼불화초산/이염화에탄 용액으로 부터 제조된 재생 셀롤로오스 섬유

  • 홍영근 (수원대학교 공과대학 고분자공학과) ;
  • 이화섭 (한국과학기술연구원 섬유고분자원연구실)
  • Published : 1992.06.01

Abstract

A mixture of trifluoroacetic acid(TFA) and methylene Chloride(MC) has been found to be an excellent solvent for cellulose. Lyotropic cellulose mesophase was obtained in 20% (w/v) solution of cellulose in this solvent system. A 16 % cellulose solution was spun into three different coagulants comprising methanol, acetone, and acetylacetone. Cellulosic filaments were successfully produced using a laboratory scale dry-jet wet spinning machine. The fibers spun had high tenacity and modulus of 3.59 and 289.1g(d, respectively. The mechanical properties of the fibers are shown to be improved comparing with those of viscose rayon.

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