고밀도, 등방성 탄소의 제조에 관한 연구

Preparation of Isotropic Carbon with High Density

  • 오종기 (한국과학기술연구원 소재화공연구실) ;
  • 이선우 (한국과학기술연구원 소재화공연구실) ;
  • 박광원 (한국과학기술연구원 신소재연구사업단)
  • 발행 : 1991.11.01

초록

The characteristics of the carbonized and calcined products made from coal tar pitch coke and coal tar pitch, were investigated in the aspect of the manufacture of isotropic graphite with high density. The mesophase from the pitch was rapidly formed at higher heat-treatment temperature between 410$^{\circ}C$ and 450$^{\circ}C$, where the insolubes in the pitch accelerated the rate of nucleation and growth of the mesophase. The benzene insolubles and the quinoline insolubes were increased as the heat treatment temperature and the heat-treatment time increased. The ratio of benzene insolubles and quinoline solubles (BI/QS) was decreased as the heat-treatment temperature was higher and maintained to be nearly constant regardless of heat-treatment time at fixed heat treatment temperature. The bulk density of the calcined carbon was linearly proportional to the ratio of quinoline solubes to volatile matter in the green coke. Anisotropic ratio of electrical resistance was measured to be between 0.98 and 1.10.

키워드

참고문헌

  1. 工學と工業 v.31 no.9 生體セラミツクス 加藤一男;靑木秀希
  2. 日本化學工學會誌 v.46 no.3 高密度, 等方性炭素材 松尾寬二
  3. 新炭素工學(改訂版) 石川敏功;長沖運
  4. J. Mater. Sci. v.16 no.1757-1762 Influence of Processed Carbon Black in the Filter Composition on the Characteristics of Baked Carbon Mixes G. Bhata;R.K. Aggarwall
  5. 日本特許公報, 昭 59207822 炭素材料の製造方法 岩矯徹
  6. Carbon v.12 no.321-333 The Formation of Mesophase Microstructures During the Pyrolysis of Selected Coker Feedstocks J.L. White;R J. Price
  7. 日本特許公報, 昭 52-108412 等方性高密度炭素材の製造方法 野田昭彦
  8. Bull. Chem. Soc. Japan v.46 no.1 Carbon Products Prepared from Variant Pitch Materials,Ⅷ. The Preparation of Isotropic Pitch Carbon with a High Density S. Otani;A. Oya
  9. 新しい工業の材料工學 A-8 一炭素と黑鉛製品一 武井武;河塢天尋
  10. ASTM D-2318, D-3175, D-4600
  11. 炭素材料工學 稻垣道夫
  12. Carbon v.12 no.307-319 Characteristics of Meso-Carbon Microbeads Separated from Pitch Y. Yamada;T. Imamura;H. Kakiyama;H. Honda;S. Oi;K. Fukuda
  13. Carbon v.3 no.185-193 The Formation of Graphitizing Carbons from the Liquid Phase J.D. Brooks;G.H. Taylor
  14. 化學工學會誌 v.27 no.5 핵산가용성분을 제거한 석탄 타르 및 핏치로부터 메조페이스 핏치의 형성 유승곤;인세진;김제영;이보성
  15. 日本窯業學會誌 v.84 no.11 低溫乾溜ピノチコ-クスを利用した等方性 · 高密度炭素材 向原進;鈴木弘茂
  16. J. Material Sci. v.17 no.525-532 Binderless Moulding of Green Cokes Delivered from Solvent Refined Coal and Ethylene Tar Pitch I. Mochida;Y. Kore;H. Fujitsu;K. Takeshita
  17. 日本化學會誌, no.12 高密度, ビノチヵ-ポソの製造とその諸性質 大谷杉郞;大谷朝男;岡田正
  18. 新炭素工業(改訂版) 石川敏功;長沖運