한국세라믹학회지 (Journal of the Korean Ceramic Society)

  • 제25권5호
  • /
  • Pages.479-487
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  • 1988
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  • 1229-7801(pISSN)
  • /
  • 2234-0491(eISSN)
한국세라믹학회 (The Korean Ceramic Society)
권호 표지

졸-겔법에 의한 실리카 유리의 제조와 DCCA로서의 Glycerol의 영향

Silica Glass Preparation by The Sol-Gel Process and The Effects of Glycerol as a DCCA

  • 이경희 (명지대학교 무기재료공학과) ;
  • 이병하 (명지대학교 무기재료공학과) ;
  • 이헌식 (삼성코닝(주) 연구소) ;
  • 오부근 (명지대학교 무기재료공학과)
  • 발행 : 1988.05.01
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초록

In this study we studied the function of Glycerol as a DCCA(Drying Control Chemical Additives) in the preparation of silica bulk glas through Sol-Gel method. We used TEOS(Tetra Ethyl Ortho Silicate) and maintained the mixing ratio of TEOS : H2O : EtOH : HCI as 1 : 4 : 4 : 0.0007(mol) and varied glycerol input quantity from 0.1vol% considering the ethnaol input quantity as 100vol%. We investigated the changes from Sol-Gel Synthetic solutions to the glass using DT-TG, FT-IR and other instruments. The results obtained from this experiment showed that the dried gels made from the synthetic solutions containing 0.1-1.0vol% of glycerol were easily heat-treated up to 85$0^{\circ}C$ so that transparant bulk silica glass was prepared.

키워드

참고문헌

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