Applied Biological Chemistry
- Volume 16 Issue 1
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- Pages.12-17
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- 1973
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- 2468-0834(pISSN)
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- 2468-0842(eISSN)
Isolation and Characterization of Alliin From Garlic Bulbs
마늘중 Alliin의 분리 및 그 특성규명에 관한 연구
- Han, In-Ja (College of Pharmacy, Ewha Womans University) ;
- Lee, Mie-Soon (Radiation Research Institute in Agriculture) ;
- Chung, Ki-Yong (College of Pharmacy, Ewha Womans University)
- Published : 1973.03.31
Abstract
Alliin was isolated from deep-frozen garlic bulbs and purified into crystalline form. Purity of isolated alliin was assured by melting point determination and thin-layer chromatography. Sulfoxide bond and functional groups of amino acid were confirmed with IR spectrum, and vinyl bond with NMR spectrum. Molecular weight, allyl and other bonds were confirmed with MS spectrum.
냉동시킨 마늘로부터 Alliin을 분리(分離)해서 순수한 상태(相態)로 결정화(結晶化) 시켰다. 분리(分離)된 Alliin의 순도(純度)는 융점측정과 thin-layer chromatography에 의하여 확증되었다. Sulfoxide bond 및 아미노산의 기능기는 IR spectrum에 의하여, vinyl 결합은 NMR spectrum에 의하여 확인되었다. 분자량, allyl 및 기타의 결합은 MS spectrum에 의하여 확인(確認)되었다.
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