Sublimatography의 V.C.P 및 물질전달에 관한 연구(I) -진공도 변화에 따른 V.C.P 와 $t_h$와의 관계-

Studied on the Mass Transfer and the Vacuum Condensing Point of Sublimatography(I) -Relations between the Heating Temperature and the V.C.P at different Degree of Vacuum-

  • 김주봉 (동아대학교 공과대학 화학공학과) ;
  • 손진언 (동아대학교 공과대학 화학공학과)
  • Kim, Joo-Bong (Dept. of Chem. Eng., College of Engineering, Dong-A University) ;
  • Sohn, Jin-Un (Dept. of Chem. Eng., College of Engineering, Dong-A University)
  • 발행 : 19701200

초록

The relation between the heating temperature and the V.C.P(Vacuum Condensing Point) at different degree of vacuum through the sublimatographic separation was studied where by ; (1) Anthracene and Anthraquinone, ${\alpha}$-Naphtol and ${\beta}$-Naphthol, o-Aminobenzoicacid and p-Aminobeenzoicacid were easily separated from each of its mixtures as shown in Figure9, 10 and 11, while tailings appeared appreciably. The results were in good agreement with those expected from the $t_k$-V.C.P curves in Figures 3,4,5,6,7 and 8. (2) The relation between the degree of vacuum and the V.C.P. of ${\alpha}$-Naphthol and Anthracene at different heating temperatures appeared as follows and are shown in Figures 12 and 13.

키워드

참고문헌

  1. Ind. Eng. Chem. v.39 D. R. Stull
  2. Natur Wiss. v.41 M. Behrens;A. Fischer
  3. J. Am. Chem. Soc. v.77 D. Gross;G. Grodsky
  4. Recent Experimental Methods in Physical Chemistry v.1 K. Kuradani;T. Shimauchi
  5. Nippon Kagaku Zassi v.80 E. Shibata;S. Saito
  6. VACUUM CHEMISTRY(Shinku Kagaku) v.8 E. Shibata
  7. Kagaku no Ryoiki v.15 E. Shibata
  8. JAPAN ANALYST(Bunseki Kagaku) v.10 E. Shibata;S. Saito
  9. Kagaku no Ryoiki v.16 K. Yamagawa
  10. JAPAN ANALYST (Bunseki Kagaku) v.11 K. Yoshimura
  11. JAPAN ANALYST (Bunseki Kagaku) v.11 K. Yoshimura
  12. JAPAN ANALYST (Bunseki Kagaku) v.11 K.Yoshimura
  13. JAPAN ANALYST (Bunseki Kagaku) v.11 K. Yoshimura
  14. VACUUM CHEMISTRY (Shinku Kagaku) v.12 S. Saito;M. Kinoshida;I. Kamii
  15. VACUUM CHEMISTRY (Shinku Kagaku) v.13 M. Kinoshida;S. Saito