Studies on Photosensitive Resins.-Molecular Weight Determination of Isophthalic Acid-Cinnamic Acid-Glycerine Polycondensates

感光性樹脂에 關한 硏究-Isophthalic acid-Cinnamic acid-Glycerine 系 縮重合物의 分子量에 關하여

  • Shim, Jyong-Sup (Department of Chemical Engineering, College of Engineering, Seoul National University) ;
  • Lee, Boo-Sop (Department of Chemical Engineering, College of Engineering, Seoul National University)
  • 심정섭 (서울大學校 工科大學 化學工學科) ;
  • 이부섭 (서울大學校 工科大學 化學工學科)
  • Published : 19620200

Abstract

The polycondensates of isophthalic acid-cinnamic acid-glycerine system were synthesized. The molecular weights of these products were determined by two methods, viscosity method and osmotic pressure methods. In the synthesis of resin, the reaction temperature was kept at 232$^{\circ}C$ and the mole ratio of the reactants was chosen as follows: Glycerine ;1.0 Isophthalic acid ;1.0 Cinnamic acid ;2.8 Excessive cinnamic acid prevented gelation of reaction mixtures. As the solution became very dilute, reduced osmotic pressure P/C (at the concentration of solution below 0.24g/100 ml of acetone) and reduced viscosity ${\eta}_{sp}/C$ (at the concentration of solution below 0.32 g/100 ml of acetone) increased rapidly. The correspondence between molecular weights determined by the two methods made Huggin's equation applicable to the prepared polymer. The values of K and a are $2.77{\times}10^{-5}$ and 1.063, respectively.

Keywords

References

  1. Ber. v.55 H. Stobbe;F.K. Steinberger
  2. Ind. Eng. Chem. v.21 R.H. Kienle;C.S. Fergus
  3. Bulletin The Chemistry and processing of Alkyd Resin Monsanto Chemical Company.
  4. Principles of Polymer Chemistry P.J. Flory
  5. J. Polymer. Science v.6 H.J. Philipp
  6. Ind. Eng. Chem. v.21 R.H. Kienle;C.S. Fergus