2nd Nanotube Formed Surface Observation of the Ti-25Ta-xZr Alloys Using ATO Technique

  • Kim, Hyun-Ju (Department of Dental Materials, Research Center of Nano-Interface Activation for Biomaterials, &Research Center for Oral Disease Regulation of the Aged, School of Dentistry, Chosun University) ;
  • Lee, Ho-Jong (Department of Materials Science and Metallurgical Engineering, Sunchon National University) ;
  • Choe, Han-Cheol (Department of Dental Materials, Research Center of Nano-Interface Activation for Biomaterials, &Research Center for Oral Disease Regulation of the Aged, School of Dentistry, Chosun University)
  • 발행 : 2013.05.30

초록

The purpose of this study was to investigate $2^{nd} $nanotube formed surface observation of the Ti-25Ta-xZr alloys using ATO(anodic titanium oxide) technique. Ti-25Ta-xZr alloy was anodized in 1M $H_3PO_4$ electrolytes containing 0.8 Wt. % NaF at room temperature. After formation of nanotube was achieved out, nanotube was eliminated, and then anodization was carried out repeatedly. The microstructures, phase transformation, and morphology of nanotubular Ti-25Ta-xZr alloys and process of nanotube growth by using ATO method was examined by optical microscopy (OM), X-ray diffraction (XRD), and field emission scanning electron microscopy (FE-SEM). The ${\alpha}$ phase and ${\beta}$ phases were affected to form the second nanotube morphology of Ti-25Ta-xZr alloys.

키워드