Proceedings of the KAIS Fall Conference (한국산학기술학회:학술대회논문집)

The Korea Academia-Industrial cooperation Society (한국산학기술학회)
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Synthesis of Ethyl 5-methylbicyclo[2.2.1]hept-2-ene-5-carboxylate

Ethyl 5-Methylbicyclo[2.2.1]hept-2-ene-5-carboxylate의 합성

  • Lee, Yoon-Bae (Dept of Chemical Engineering, Soonchunhyang University) ;
  • Jun, Joon-Ho (Dept of Chemical Engineering, Soonchunhyang University) ;
  • Yoo, Jin-Yi (Dept of Chemical Engineering, Soonchunhyang University) ;
  • Sung, Un-Gyung (Dept of Chemical Engineering, Soonchunhyang University)
  • 이윤배 (순천향대학교 화학공학과) ;
  • 전준호 (순천향대학교 화학공학과) ;
  • 유진이 (순천향대학교 화학공학과) ;
  • 성언경 (순천향대학교 화학공학과)
  • Published : 2008.05.22
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Abstract

Ethyl methacrylate와 cyclopentadiene을 반응하여 Ethyl 5-methylbicyclo[2.2.1]hept-2-ene-5-carboxylate (EMBHC)를 합성하고 만들어진 EMBHC를 Column Chromatography를 이용하여 endo와 exo를 분리해 GC를 이용하여 그 비율을 측정하였고 $^1H$-NMR을 이용하여 endo와 exo 화합물의 구조를 확인하였다.

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