한국지하수토양환경학회:학술대회논문집 (Proceedings of the Korean Society of Soil and Groundwater Environment Conference)
- 한국지하수토양환경학회 2005년도 총회 및 춘계학술발표회
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- Pages.195-198
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- 2005
기체크로마토그래피-질량분석검출기와 고체상미량추출법을 이용한 물 중의 MTBE 미량분석
- 발행 : 2005.04.01
초록
A solid-phase microextraction and gas chromatography-mass spectrometry for the extraction and analysis of methyl-tert-butyl ether has been described. methyl-tert-butyl ether was extracted from aqueous solution using SPME fiber coated polydimethylsiloxane and analysed by GC-MS with capillary column. Extraction parameters and chromatographic separation conditions were optimized. The applied method represented good analytical performance in terms of precision (3-8%, RSD) and accuracy(93-102%, mean recovery) with a method detection limit of 0.03 ppb.