Proceedings of the PSK Conference (대한약학회:학술대회논문집)

The Pharmaceutical Society of Korea (대한약학회)
권호 표지

Simultaneous determination of nalbuphine and methamphetamine in drug abuser's urine

  • Park, Mee-Jung (Dept of Forensic science, National Institute of Scientific Investigation) ;
  • Choi, Wha-Kyung (Dept of Forensic science, National Institute of Scientific Investigatio) ;
  • Choi, Sang-Kil (Dept of Forensic science, National Institute of Scientific Investigatio) ;
  • Son, Haeng-Ja (Dept of Forensic science, National Institute of Scientific Investigatio) ;
  • Lim, Mi-Ae (Dept of Forensic science, National Institute of Scientific Investigatio) ;
  • Chung, Hee-Sun (Dept of Forensic science, National Institute of Scientific Investigation)
  • Published : 2003.04.01
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Abstract

Because people who take more than two drugs have increases, a simple and sensitive method for the simultaneous analysis of amphetamine, methamphetamine and nalbuphine in urine was developed. After alkalinization of the urine samples with 6 N-NaOH, the analytes were extracted using ethyl acetate, derivatized with MSTFA : TSIM : TMCS (= 100 : 2 : 5) prior to gas chromatography-mass spectrometry(GC-MS) analysis with selected ion monitoring. (omitted)

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