Synthesis of Langasite Powder by a Chemical Route

  • Kim, Kyoung-Jin (Department of ceramic engineering, Hanyang University) ;
  • Kim, Jung-Hwan (Department of ceramic engineering, Hanyang University) ;
  • Kim, Young-Do (Department of Materials Science and Engineering, Kanwon National University) ;
  • Joo, Kwang-Suk (Department of Materials Science and Engineering, Kanwon National University) ;
  • Shin, Kun-Chul (Ceramic Processing Research Center, Hanyang University) ;
  • Auh, Keun-Ho (Ceramic Processing Research Center, Hanyang University)
  • 발행 : 1998.06.01

초록

Langasite({{{{ { La}_{ 3} {Ga }_{5 } {SiO }_{14 } , LGS}}}}) powder was prepared by a polymerized complex method based on the Pechini-type reaction. A mixed solution of ethylene glycol(EG), cotric acid(CA), lanthanum, gallium and silicon ions, with a molar ratio of EG:CA:La:Ga:Si=100:25:3:5:1, was polymerzed to from a transparent resin, which was used as a precursor for the synthesis of LGS. X-ray diffraction(XRD) patterns indicated that the LGS phase could be formed by the heat-treatment in air at 1000$^{\circ}C$ for 3hrs

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